Investigation by TGA-FTIR of the effect of styrene content and thickness on the UV-curing of vinylester resins

Article

Cardona, F., Rogers, D. and Van Erp, G.. 2007. "Investigation by TGA-FTIR of the effect of styrene content and thickness on the UV-curing of vinylester resins." Journal of Thermoplastic Composite Materials. 20 (6), pp. 601-615. https://doi.org/10.1177/0892705707083950
Article Title

Investigation by TGA-FTIR of the effect of styrene content and thickness on the UV-curing of vinylester resins

ERA Journal ID4954
Article CategoryArticle
AuthorsCardona, F. (Author), Rogers, D. (Author) and Van Erp, G. (Author)
Journal TitleJournal of Thermoplastic Composite Materials
Journal Citation20 (6), pp. 601-615
Number of Pages15
Year2007
PublisherSAGE Publications Ltd
Place of PublicationThousand Oaks, CA. United States
ISSN0892-7057
1530-7980
Digital Object Identifier (DOI)https://doi.org/10.1177/0892705707083950
Web Address (URL)http://jtc.sagepub.com/content/20/6/601.full.pdf+html
Abstract

The influence of styrene content and thickness of the samples on the UV curing of Vinyl ester/Styrene resins (VERs) was investigated by DSC and the combination of TGA and FT-IR (TGA-FTIR). The glass transition temperatures of the network polymers after curing were found to be lower for the VERs with higher styrene content. The released heat during UV curing further increased the Tg, with this increase being proportional to the volume of the resins. Within the range of thickness investigated (up to 30 mm) the relative amount of emissions of ST, VE and CO2 were found to be the similar at the top and at the bottom of the samples. Similar results were obtained from the TGA analysis, indicating that the VERs were fully or almost fully cured all along the cross section. A good correlation was found between the analysis of the thermal properties by DSC and the results obtained by the TGA-FTIR system.

KeywordsTGA-FTIR; styrene; vinylester; UV curing; Tg; heat released; crosslink density
ANZSRC Field of Research 2020400505. Construction materials
401602. Composite and hybrid materials
401609. Polymers and plastics
Public Notes

File reproduced in accordance with the copyright policy of the publisher/author.

Byline AffiliationsCentre of Excellence in Engineered Fibre Composites
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Brell, Edward, Van Erp, Gerard and Snook, Chris. 2002. "Train crashworthiness and its impact on society." Australian Journal of Mechanical Engineering. 25 (2), pp. 103-112.
Fibre composite bridge decks: an alternative approach
Davey, Scott W., Van Erp, Gerard M. and Marsh, Roy. 2001. "Fibre composite bridge decks: an alternative approach." Composites Part A: Applied Science and Manufacturing. 32 (9), pp. 1339 - 1343. https://doi.org/10.1016/S1359-835X(01)00087-2
A Code of Practice for the structural design of fibre composites
Ayers, Stephen R. and van Erp, Gerard. 2004. "A Code of Practice for the structural design of fibre composites ." Proceedings of the Institution of Civil Engineers: Structures and Buildings. 157 (1), pp. 3-8. https://doi.org/10.1680/stbu.157.1.3.36408
Studies on polymers and composites from lignin and fiber derived from sugar cane
Doherty, William, Halley, Peter J., Edye, Les, Rogers, David, Cardona, Francisco, Park, Yosup and Woo, Tim. 2007. "Studies on polymers and composites from lignin and fiber derived from sugar cane." Polymers for Advanced Technologies. 18 (8), pp. 673-678. https://doi.org/10.1002/pat.879
Investigation of the effect of styrene content on the ultimate curing of vinylester resins by TGA-FTIR
Cardona, F., Rogers, D., Davey, S. and Van Erp, G.. 2007. "Investigation of the effect of styrene content on the ultimate curing of vinylester resins by TGA-FTIR." Journal of Composite Materials. 41 (2), pp. 137-152. https://doi.org/10.1177/002199830?063357
Plant based resins for fibre composites
Faigl, Pavel, Rogers, David, Maurin, Romain and Van Erp, Gerard. 2007. "Plant based resins for fibre composites." 4th Annual Composites Australia and Composites CRC Conference (CRC 2007): New Technology Taking Shape. Gold Coast, Australia 19 - 20 Apr 2007 Melbourne, Australia.
Fracture toughness of phenol formaldehyde composites post-cured in microwaves
Cardona, F., Ku, H., Pattarachaiyakoop, N., Rogers, D. and Trada, M.. 2007. "Fracture toughness of phenol formaldehyde composites post-cured in microwaves." Journal of Electromagnetic Waves and Applications. 21 (14), pp. 2137-2146. https://doi.org/10.1163/156939307783152867
Stressed arch modular deployable composite shelters: concept and development
Omar, T., Van Erp, G. and Key, P. W.. 2006. "Stressed arch modular deployable composite shelters: concept and development ." Mirmiran, A. and Nanni, A. (ed.) CICE 2006: 3rd International Conference on FRP Composites in Civil Engineering. Miami, United States 13 - 15 Dec 2006 Miami, Fl, USA.
Modular deployable composite shelters - truss system
Omar, T., Van Erp, G. and Key, P.. 2007. "Modular deployable composite shelters - truss system ." Darby, A. P. and Ibell, T. P. (ed.) ACIC 2007: Advanced Composites in Construction Conference . Bath, United Kingdom 02 - 04 Apr 2007 York, UK.
M2S2 modular deployable composite shelters: concept and loading criteria
Omar, Tarek, Heldt, Tim, Key, P. and Van Erp, Gerard. 2006. "M2S2 modular deployable composite shelters: concept and loading criteria." Australian Journal of Structural Engineering. 6 (3), pp. 217-226.
Design and analysis of a composite beam for infrastructure applications - Part III: experimental results and nonlinear FE analysis
Springolo, Mario, Khennane, Amar and Van Erp, Gerard. 2006. "Design and analysis of a composite beam for infrastructure applications - Part III: experimental results and nonlinear FE analysis ." International Journal of Materials and Product Technology. 25 (4), pp. 331-347.
Design and analysis of a composite beam for infrastructure applications - Part II: preliminary investigation in shear and torsion
Springolo, Mario, Van Erp, Gerard and Khennane, Amar. 2006. "Design and analysis of a composite beam for infrastructure applications - Part II: preliminary investigation in shear and torsion ." International Journal of Materials and Product Technology. 25 (4), pp. 313-331.
Design and analysis of a composite beam for infrastructure applications - Part I: preliminary investigation in bending
Springolo, Mario, Van Erp, Gerard and Khennane, Amar. 2006. "Design and analysis of a composite beam for infrastructure applications - Part I: preliminary investigation in bending ." International Journal of Materials and Product Technology. 25 (4), pp. 297-313. https://doi.org/10.1504/IJMPT.2006.008885
Vinylester/cenosphere composite materials for civil and structural engineering
Davey, Scott W., Heldt, Tim, Van Erp, Gerard and Ayers, Stephen R.. 2005. "Vinylester/cenosphere composite materials for civil and structural engineering." FRP International : The Official Newsletter of the International Institute for FRP in Construction. 2 (3), pp. 2-5.
Development of modular deployable composite shelters
Omar, T., Heldt, T., Key, P. and Van Erp, G.. 2005. "Development of modular deployable composite shelters." Stewart, Mark G. and Dockrill, Brad (ed.) 2005 Australian Structural Engineering Conference (ASEC 2005). Newcastle, Australia 11 - 14 Sep 2005 Sydney, Australia.
Train crashworthiness and its impact on society
Brell, Edward, Van Erp, Gerard and Snook, Chris. 1999. "Train crashworthiness and its impact on society." International Journal of Crashworthiness. 4 (4), pp. 419-431. https://doi.org/10.1533/cras.1999.0116