Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption

Article

Sun, Jiajia, Wang, Chengrui, Zeng, Li, Xu, Pengfei, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Jin, Quan and Yu, Ranbo. 2016. "Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption." Materials Research Bulletin. 75, pp. 110-114. https://doi.org/10.1016/j.materresbull.2015.11.035
Article Title

Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption

ERA Journal ID4969
Article CategoryArticle
AuthorsSun, Jiajia (Author), Wang, Chengrui (Author), Zeng, Li (Author), Xu, Pengfei (Author), Yang, Xiaodan (Author), Chen, Jun (Author), Xing, Xianran (Author), Jin, Quan (Author) and Yu, Ranbo (Author)
Journal TitleMaterials Research Bulletin
Journal Citation75, pp. 110-114
Number of Pages5
Year2016
PublisherElsevier
Place of PublicationUnited Kingdom
ISSN0025-5408
1873-4227
Digital Object Identifier (DOI)https://doi.org/10.1016/j.materresbull.2015.11.035
Web Address (URL)http://www.sciencedirect.com/science/article/pii/S0025540815302282?via%3Dihub
Abstract

CeO2 micro/nanospheres with perfect spherical morphology, large specific surface area, high porosity, high stability and adjustable diameter were hydrothermally synthesized from a simple system, and the stirring-time before hydrothermal process was found to be the key factor for the final particle size control. The CeO2 spheres with diameters from ∼800 nm to ∼50 nm could be harvested by controllable synthesis. And the highest specific surface area of these CeO2 spheres could achieve 182 m2 g-1. Moreover, CeO2 spheres with higher specific surface areas (182 m2 g-1 and 117 m2 g-1) showed excellent performance in removal of heavy metal ion Cr(VI) from the aqueous solution. The Cr(VI) removal efficiencies could reach up to 94%.

KeywordsChemical synthesis; Inorganic compounds; Nanostructures; Oxides; Solvothermal; Controllable synthesis; Cr adsorptions; Hydrothermal process; Hydrothermally synthesized; Large specific surface areas; Particle size control; Solvothermal; Spherical morphologies; Metallurgy and Metallography; Metallurgy; Nanotechnology; Chemical Reactions; Chemical Products Generally; Inorganic Compounds; Solid State Physics;
ANZSRC Field of Research 2020401699. Materials engineering not elsewhere classified
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Byline AffiliationsUniversity of Science and Technology Beijing, China
Chinese Academy of Sciences, China
Institution of OriginUniversity of Southern Queensland
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An, Xiaoxin, Wang, You, Deng, Jinxia, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2014. "One step molten salt synthesis of YVO4 nanoparticles and their photocatalytic properties under UV-Visible light." Inorganic Chemistry Communications. 44, pp. 79-82. https://doi.org/10.1016/j.inoche.2014.03.010
A low-cost and large-scale synthesis of nano-zinc oxide from smithsonite
Zhang, Yucheng, Deng, Jinxia, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2014. "A low-cost and large-scale synthesis of nano-zinc oxide from smithsonite." Inorganic Chemistry Communications. 43, pp. 138-141. https://doi.org/10.1016/j.inoche.2014.02.032
Quintuple-shelled Sno2 hollow microspheres with superior light scattering for high-performance dye-sensitized solar cells
Dong, Zhenghong, Ren, Hao, Hessel, Colin M., Wang, Jiangyan, Yu, Ranbo, Jin, Quan, Yang, Mei, Hu, Zhudong, Chen, Yunfa, Tang, Zhiyong, Zhao, Huijun and Wang, Dan. 2014. "Quintuple-shelled Sno2 hollow microspheres with superior light scattering for high-performance dye-sensitized solar cells." Advanced Materials. 26 (6), pp. 905-909. https://doi.org/10.1002/adma.201304010
Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing
Wang, You, Wang, Yun, Chen, Jun, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2015. "Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing." European Journal of Inorganic Chemistry. 2015 (35), pp. 5767-5772. https://doi.org/10.1002/ejic.201500869
Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries
Wang, Feng, Wang, Jiangyan, Ren, Hao, Tang, Hongjie, Yu, Ranbo and Wang, Dan. 2016. "Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries." Inorganic Chemistry Frontiers. 3 (3), pp. 365-369. https://doi.org/10.1039/c5qi00213c
Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor
Yan, Xuecheng, Yu, Ranbo, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2011. "Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor." Solid State Sciences. 13 (5), pp. 1060-1064. https://doi.org/10.1016/j.solidstatesciences.2011.01.019
The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds
Chen, Jun, Nittala, Krishna, Forrester, Jennifer S., Jones, Jacob L., Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2011. "The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds." Journal of the American Chemical Society. 133 (29), pp. 11114-11117. https://doi.org/10.1021/ja2046292
Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders
Deng, Jinxia, Li, Lihong, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2012. "Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders." Inorganic Chemistry Communications. 21, pp. 92-95. https://doi.org/10.1016/j.inoche.2012.04.021
Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres
Yan, Xuecheng, Yu, Ranbo, Xu, Yali, Li, Li, Xu, Pengfei, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2012. "Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres." Materials Research Bulletin. 47 (9), pp. 2135-2139. https://doi.org/10.1016/j.materresbull.2012.06.013
Rapid molten salt synthesis of isotropic negative thermal expansion ScF3
Hu, Lei, Chen, Jun, Fan, Longlong, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Rapid molten salt synthesis of isotropic negative thermal expansion ScF3." Journal of the American Ceramic Society. 97 (4), pp. 1009-1011. https://doi.org/10.1111/jace.12855
Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method
Hu, Lei, Chen, Jun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method." Journal of the American Ceramic Society. 97 (5), pp. 1386-1388. https://doi.org/10.1111/jace.12932
Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range
Hu, Lei, Chen, Jun, Fan, Longlong, Ren, Yang, Rong, Yangchun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range." Journal of the American Chemical Society. 136 (39), pp. 13566-13569. https://doi.org/10.1021/ja5077487
Controlled synthesis and properties of porous Cu/CeO2 microspheres
Yao, Xiang, Yang, Xiaodan, Yu, Ranbo, Xu, Pengfei, Chen, Jun and Xing, Xianran. 2015. "Controlled synthesis and properties of porous Cu/CeO2 microspheres." Materials Research Bulletin. 61, pp. 22-25. https://doi.org/10.1016/j.materresbull.2014.09.083
N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures
Bao, Jinrong, Zhu, Xiaowei, Liu, Ying, Li, Wenxian and Yu, Ranbo. 2014. "N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures." Materials Letters. 124, pp. 97-100. https://doi.org/10.1016/j.matlet.2014.03.014
Microstructure construction and composition modification of CeO2 macrospheres with superior performance
Jiang, Shuaiyu, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Microstructure construction and composition modification of CeO2 macrospheres with superior performance." Inorganic Chemistry Frontiers. 3 (1), pp. 92-96. https://doi.org/10.1039/c5qi00140d
Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity
Cui, Pengzhen, Wang, Jiali, Wang, Zumin, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity." Nano Research. 9 (3), pp. 593-601. https://doi.org/10.1007/s12274-015-0939-z
A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite
Wang, Shuo, Yi, Luoxin, Halpert, Jonathan E., Lai, Xiaoyong, Liu, Yuanyuan, Cao, Hongbin, Wang, Dan, Yu, Ranbo and Li, Yuliang. 2012. "A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite." Small. 8 (2), pp. 265-271. https://doi.org/10.1002/smll.201101686
Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays
Ge, Lei, Chen, Jiuling, Chen, Jun, Zhu, Zhonghua and Rudolph, Victor. 2012. "Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays." Journal of Nanoscience and Nanotechnology. 12 (3), pp. 2722-2732. https://doi.org/10.1166/jnn.2012.5726
Embeddable and locatable spinning
Xu, Weilin, Xia, Zhigang, Wang, Xin, Chen, Jun, Cui, Weigang, Ye, Wenxiang, Ding, Cailing and Wang, Xungai. 2011. "Embeddable and locatable spinning." Textile Research Journal. 81 (3), pp. 223-229. https://doi.org/10.1177/0040517510380780