Low temperature molten salt synthesis of perovskite-type ACeO3(A=Sr, Ba) in eutectic NaCl-KCl

Article

Liu, Ming, Hu, Lei, Xu, Pengfei, Zhao, Kun, Zong, Lingbo, Yu, Ranbo, Chen, Jun and Xing, Xianran. 2015. "Low temperature molten salt synthesis of perovskite-type ACeO3(A=Sr, Ba) in eutectic NaCl-KCl." Chemical Research in Chinese Universities. 31 (3), pp. 342-346. https://doi.org/10.1007/s40242-015-4330-0

Article Title	Low temperature molten salt synthesis of perovskite-type ACeO3(A=Sr, Ba) in eutectic NaCl-KCl
ERA Journal ID	124562
Article Category	Article
Authors	Liu, Ming (Author), Hu, Lei (Author), Xu, Pengfei (Author), Zhao, Kun (Author), Zong, Lingbo (Author), Yu, Ranbo (Author), Chen, Jun (Author) and Xing, Xianran (Author)
Journal Title	Chemical Research in Chinese Universities
Journal Citation	31 (3), pp. 342-346
Number of Pages	5
Year	2015
Place of Publication	China
ISSN	1005-9040
	2210-3171
Digital Object Identifier (DOI)	https://doi.org/10.1007/s40242-015-4330-0
Web Address (URL)	https://link.springer.com/article/10.1007/s40242-015-4330-0
Abstract	A molten salt method was developed for the synthesis of ACeO3(A=Sr, Ba) with perovskite structure at 750 °C(SrCeO3) and 850 °C(BaCeO3) in the eutectic NaCl-KCl. The synthetic temperature was much lower than that of the conventional method(generally>1000 °C). The structure and morphology of the product were characterized by means of X-ray diffraction(XRD), field emission scanning electron microscopy(FESEM) and transmission electron microscopy(TEM). The results show that the synthesized octahedral SrCeO3 crystallizes in the orthorhombic system with the unit cell parameters of a=0.85855 nm, b=0.61523 nm, c=0.60059 nm, and the synthesized cuboid BaCeO3 crystallizes in the cubic system with the unit cell parameter of a=0.43962 nm. The result of X-ray photoelectron spectroscopy(XPS) analysis indicates that both Ce4+ and Ce3+ exist in the two structures, and the Ce4+/Ce3+ peak area ratios for SrCeO3 and BaCeO3 are 1.93 and 2.12, respectively. Meanwhile, the adsorbed/lattice oxygen ratios(1.87 for SrCeO3 and 3.04 for BaCeO3) indicate the existence of a lot of oxygen vacancies in the structures of SrCeO3 and BaCeO3, which indicates a far-reaching significance to study the corresponding physicochemistry performance.
Keywords	BaCeO3; Molten salt synthesis; Perovskite; SrCeO3;
ANZSRC Field of Research 2020	340210. Solid state chemistry
Public Notes	Files associated with this item cannot be displayed due to copyright restrictions.
Byline Affiliations	University of Science and Technology Beijing, China
Institution of Origin	University of Southern Queensland

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An, Xiaoxin, Wang, You, Deng, Jinxia, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2014. "One step molten salt synthesis of YVO4 nanoparticles and their photocatalytic properties under UV-Visible light." Inorganic Chemistry Communications. 44, pp. 79-82. https://doi.org/10.1016/j.inoche.2014.03.010

A low-cost and large-scale synthesis of nano-zinc oxide from smithsonite

Zhang, Yucheng, Deng, Jinxia, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2014. "A low-cost and large-scale synthesis of nano-zinc oxide from smithsonite." Inorganic Chemistry Communications. 43, pp. 138-141. https://doi.org/10.1016/j.inoche.2014.02.032

Quintuple-shelled Sno2 hollow microspheres with superior light scattering for high-performance dye-sensitized solar cells

Dong, Zhenghong, Ren, Hao, Hessel, Colin M., Wang, Jiangyan, Yu, Ranbo, Jin, Quan, Yang, Mei, Hu, Zhudong, Chen, Yunfa, Tang, Zhiyong, Zhao, Huijun and Wang, Dan. 2014. "Quintuple-shelled Sno2 hollow microspheres with superior light scattering for high-performance dye-sensitized solar cells." Advanced Materials. 26 (6), pp. 905-909. https://doi.org/10.1002/adma.201304010

Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing

Wang, You, Wang, Yun, Chen, Jun, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2015. "Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing." European Journal of Inorganic Chemistry. 2015 (35), pp. 5767-5772. https://doi.org/10.1002/ejic.201500869

Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries

Wang, Feng, Wang, Jiangyan, Ren, Hao, Tang, Hongjie, Yu, Ranbo and Wang, Dan. 2016. "Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries." Inorganic Chemistry Frontiers. 3 (3), pp. 365-369. https://doi.org/10.1039/c5qi00213c

Phase transformation and negative thermal expansion in TaVO5

Wang, Xiaowei, Huang, Qingzhen, Deng, Jinxia, Yu, Ranbo, Chen, Jun and Xing, Xianran. 2011. "Phase transformation and negative thermal expansion in TaVO5." Inorganic Chemistry: including bioinorganic chemistry. 50 (6), pp. 2685-2690. https://doi.org/10.1021/ic200003n

Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor

Yan, Xuecheng, Yu, Ranbo, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2011. "Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor." Solid State Sciences. 13 (5), pp. 1060-1064. https://doi.org/10.1016/j.solidstatesciences.2011.01.019

The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds

Chen, Jun, Nittala, Krishna, Forrester, Jennifer S., Jones, Jacob L., Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2011. "The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds." Journal of the American Chemical Society. 133 (29), pp. 11114-11117. https://doi.org/10.1021/ja2046292

Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders

Deng, Jinxia, Li, Lihong, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2012. "Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders." Inorganic Chemistry Communications. 21, pp. 92-95. https://doi.org/10.1016/j.inoche.2012.04.021

Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres

Yan, Xuecheng, Yu, Ranbo, Xu, Yali, Li, Li, Xu, Pengfei, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2012. "Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres." Materials Research Bulletin. 47 (9), pp. 2135-2139. https://doi.org/10.1016/j.materresbull.2012.06.013

Rapid molten salt synthesis of isotropic negative thermal expansion ScF3

Hu, Lei, Chen, Jun, Fan, Longlong, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Rapid molten salt synthesis of isotropic negative thermal expansion ScF3." Journal of the American Ceramic Society. 97 (4), pp. 1009-1011. https://doi.org/10.1111/jace.12855

Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method

Hu, Lei, Chen, Jun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method." Journal of the American Ceramic Society. 97 (5), pp. 1386-1388. https://doi.org/10.1111/jace.12932

Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range

Hu, Lei, Chen, Jun, Fan, Longlong, Ren, Yang, Rong, Yangchun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range." Journal of the American Chemical Society. 136 (39), pp. 13566-13569. https://doi.org/10.1021/ja5077487

Controlled synthesis and properties of porous Cu/CeO2 microspheres

Yao, Xiang, Yang, Xiaodan, Yu, Ranbo, Xu, Pengfei, Chen, Jun and Xing, Xianran. 2015. "Controlled synthesis and properties of porous Cu/CeO2 microspheres." Materials Research Bulletin. 61, pp. 22-25. https://doi.org/10.1016/j.materresbull.2014.09.083

Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption

Sun, Jiajia, Wang, Chengrui, Zeng, Li, Xu, Pengfei, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Jin, Quan and Yu, Ranbo. 2016. "Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption." Materials Research Bulletin. 75, pp. 110-114. https://doi.org/10.1016/j.materresbull.2015.11.035

N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures

Bao, Jinrong, Zhu, Xiaowei, Liu, Ying, Li, Wenxian and Yu, Ranbo. 2014. "N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures." Materials Letters. 124, pp. 97-100. https://doi.org/10.1016/j.matlet.2014.03.014

Microstructure construction and composition modification of CeO2 macrospheres with superior performance

Jiang, Shuaiyu, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Microstructure construction and composition modification of CeO2 macrospheres with superior performance." Inorganic Chemistry Frontiers. 3 (1), pp. 92-96. https://doi.org/10.1039/c5qi00140d

Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity

Cui, Pengzhen, Wang, Jiali, Wang, Zumin, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity." Nano Research. 9 (3), pp. 593-601. https://doi.org/10.1007/s12274-015-0939-z

A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite

Wang, Shuo, Yi, Luoxin, Halpert, Jonathan E., Lai, Xiaoyong, Liu, Yuanyuan, Cao, Hongbin, Wang, Dan, Yu, Ranbo and Li, Yuliang. 2012. "A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite." Small. 8 (2), pp. 265-271. https://doi.org/10.1002/smll.201101686

Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays

Ge, Lei, Chen, Jiuling, Chen, Jun, Zhu, Zhonghua and Rudolph, Victor. 2012. "Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays." Journal of Nanoscience and Nanotechnology. 12 (3), pp. 2722-2732. https://doi.org/10.1166/jnn.2012.5726

Embeddable and locatable spinning

Xu, Weilin, Xia, Zhigang, Wang, Xin, Chen, Jun, Cui, Weigang, Ye, Wenxiang, Ding, Cailing and Wang, Xungai. 2011. "Embeddable and locatable spinning." Textile Research Journal. 81 (3), pp. 223-229. https://doi.org/10.1177/0040517510380780

Low temperature molten salt synthesis of perovskite-type ACeO3(A=Sr, Ba) in eutectic NaCl-KCl

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