A general and rapid synthesis of metal sulphides hollow spheres that have properties enhanced by salt-assisted aerosol decomposition: a case of ZnS and other multicomponent solid solutions

Article

Zou, Wei, Chen, Jun, Hu, Lei, Li, Qiang, Yao, Xiang, Gu, Lin, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "A general and rapid synthesis of metal sulphides hollow spheres that have properties enhanced by salt-assisted aerosol decomposition: a case of ZnS and other multicomponent solid solutions." Journal of Materials Chemistry C. 2 (40), pp. 8564-8568. https://doi.org/10.1039/c4tc01557f
Article Title

A general and rapid synthesis of metal sulphides hollow spheres that have properties enhanced by salt-assisted aerosol decomposition: a case of ZnS and other multicomponent solid solutions

ERA Journal ID201060
Article CategoryArticle
AuthorsZou, Wei (Author), Chen, Jun (Author), Hu, Lei (Author), Li, Qiang (Author), Yao, Xiang (Author), Gu, Lin (Author), Deng, Jinxia (Author), Yu, Ranbo (Author) and Xing, Xianran (Author)
Journal TitleJournal of Materials Chemistry C
Journal Citation2 (40), pp. 8564-8568
Number of Pages5
Year2014
PublisherThe Royal Society of Chemistry
Place of PublicationUnited Kingdom
ISSN2050-7526
2050-7534
Digital Object Identifier (DOI)https://doi.org/10.1039/c4tc01557f
Web Address (URL)http://pubs.rsc.org/-/content/articlelanding/2014/tc/c4tc01557f#!divAbstract
Abstract

Synthesis of hollow structures of metal sulphides generally involves various templates and complex chemical processing. In the present study, a general and rapid method of salt-assisted aerosol decomposition (SAD) is presented for the synthesis of hollow spheres of various metal sulfides, including ZnS, ternary sulfides, and solid solutions. The NaCl salt plays a critical role in the formation of hollow spheres of metal sulfides. The hollow spherical microstructure was formed from solid by using a small amount of water soluble NaCl salt. The formation of metal sulphide hollow spheres differs from previous mechanisms and is referred to as molten salt heterogeneous nucleation (MSHN). The present method offers the most promising advantage for controlling the multicomponent composition of hollow spheres. Furthermore, hollow spheres of sulphides have much enhanced properties such as photoluminescence of ZnS:Mn2+and photocatalytic dye degradation of ZnIn2S4due to the role of molten salt in the promotion of crystallization, The present method could be explored further by applying the process to other compounds such as sulfides, oxides, and nitrides.

KeywordsHollow sphere; Multicomponent solid solutions; Rapid synthesis; Salt-assisted; FLUIDEX
ANZSRC Field of Research 2020340211. Transition metal chemistry
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Byline AffiliationsUniversity of Science and Technology Beijing, China
Chinese Academy of Sciences, China
Institution of OriginUniversity of Southern Queensland
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https://research.usq.edu.au/item/q4268/a-general-and-rapid-synthesis-of-metal-sulphides-hollow-spheres-that-have-properties-enhanced-by-salt-assisted-aerosol-decomposition-a-case-of-zns-and-other-multicomponent-solid-solutions

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Ren, Hao, Sun, Jiajia, Yu, Ranbo, Yang, Mei, Gu, Lin, Liu, Porun, Zhao, Huijun, Kisailus, David and Wang, Dan. 2015. "Controllable synthesis of mesostructures from TiO2 hollow to porous nanospheres with superior rate performance for lithium ion batteries." Chemical Science. 7 (1), pp. 793-798. https://doi.org/10.1039/c5sc03203b
Multiple Au cores in CeO2 hollow spheres for the superior catalytic reduction of p-nitrophenol
Zhao, Kun, Qi, Jian, Zhao, Shenlong, Tang, Hongjie, Yin, Huajie, Zong, Lingbo, Chang, Lin, Gao, Yan, Yu, Ranbo and Tang, Zhiyong. 2015. "Multiple Au cores in CeO2 hollow spheres for the superior catalytic reduction of p-nitrophenol." Chinese Journal of Catalysis. 36 (3), pp. 261-267. https://doi.org/10.1016/S1872-2067(14)60273-4
Y203:Yb3+/Er3+ hollow spheres with controlled inner structures and enhanced upconverted photoluminescence
Zong, Lingbo, Xu, Pengfei, Ding, Yunji, Zhao, Kun, Wang, Zumin, Yan, Xuecheng, Yu, Ranbo, Chen, Jun and Xing, Xianran. 2015. "Y203:Yb3+/Er3+ hollow spheres with controlled inner structures and enhanced upconverted photoluminescence." Small. 11 (23), pp. 2768-2773. https://doi.org/10.1002/smll.201402320
Controlled synthesis of tetragonal terbium orthophosphate nanostructures through a solvothermal route
Yu, Ranbo, Bao, Jinrong, Yang, Xiaodan, Zhang, Jiayun, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2011. "Controlled synthesis of tetragonal terbium orthophosphate nanostructures through a solvothermal route." Research on Chemical Intermediates. 37 (2-5), pp. 145-151. https://doi.org/10.1007/s11164-011-0261-7
Hierarchical hydroxyapatite microspheres composed of nanorods and their competitive sorption behavior for heavy metal ions
Zhu, Ronghai, Lai, Xiaoyong, Halpert, Jonathan E., Yu, Ranbo and Wang, Dan. 2012. "Hierarchical hydroxyapatite microspheres composed of nanorods and their competitive sorption behavior for heavy metal ions." European Journal of Inorganic Chemistry. https://doi.org/10.1002/ejic.201101038
Water-soluble monodispersed lanthanide oxide submicrospheres: PVP-assisted hydrothermal synthesis, size-control and luminescence properties
Cui, Ying, Lai, Xiaoyong, Li, Li, Hu, Zhudong, Wang, Shuo, Halpert, Jonathan E., Yu, Ranbo and Wang, Dan. 2012. "Water-soluble monodispersed lanthanide oxide submicrospheres: PVP-assisted hydrothermal synthesis, size-control and luminescence properties." ChemPhysChem: a European journal of chemical physics and physical chemistry. 13 (10), pp. 2610-2614. https://doi.org/10.1002/cphc.201100806
One step molten salt synthesis of YVO4 nanoparticles and their photocatalytic properties under UV-Visible light
An, Xiaoxin, Wang, You, Deng, Jinxia, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2014. "One step molten salt synthesis of YVO4 nanoparticles and their photocatalytic properties under UV-Visible light." Inorganic Chemistry Communications. 44, pp. 79-82. https://doi.org/10.1016/j.inoche.2014.03.010
A low-cost and large-scale synthesis of nano-zinc oxide from smithsonite
Zhang, Yucheng, Deng, Jinxia, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2014. "A low-cost and large-scale synthesis of nano-zinc oxide from smithsonite." Inorganic Chemistry Communications. 43, pp. 138-141. https://doi.org/10.1016/j.inoche.2014.02.032
Quintuple-shelled Sno2 hollow microspheres with superior light scattering for high-performance dye-sensitized solar cells
Dong, Zhenghong, Ren, Hao, Hessel, Colin M., Wang, Jiangyan, Yu, Ranbo, Jin, Quan, Yang, Mei, Hu, Zhudong, Chen, Yunfa, Tang, Zhiyong, Zhao, Huijun and Wang, Dan. 2014. "Quintuple-shelled Sno2 hollow microspheres with superior light scattering for high-performance dye-sensitized solar cells." Advanced Materials. 26 (6), pp. 905-909. https://doi.org/10.1002/adma.201304010
Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing
Wang, You, Wang, Yun, Chen, Jun, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2015. "Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing." European Journal of Inorganic Chemistry. 2015 (35), pp. 5767-5772. https://doi.org/10.1002/ejic.201500869
Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries
Wang, Feng, Wang, Jiangyan, Ren, Hao, Tang, Hongjie, Yu, Ranbo and Wang, Dan. 2016. "Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries." Inorganic Chemistry Frontiers. 3 (3), pp. 365-369. https://doi.org/10.1039/c5qi00213c
Phase transformation and negative thermal expansion in TaVO5
Wang, Xiaowei, Huang, Qingzhen, Deng, Jinxia, Yu, Ranbo, Chen, Jun and Xing, Xianran. 2011. "Phase transformation and negative thermal expansion in TaVO5." Inorganic Chemistry: including bioinorganic chemistry. 50 (6), pp. 2685-2690. https://doi.org/10.1021/ic200003n
Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor
Yan, Xuecheng, Yu, Ranbo, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2011. "Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor." Solid State Sciences. 13 (5), pp. 1060-1064. https://doi.org/10.1016/j.solidstatesciences.2011.01.019
The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds
Chen, Jun, Nittala, Krishna, Forrester, Jennifer S., Jones, Jacob L., Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2011. "The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds." Journal of the American Chemical Society. 133 (29), pp. 11114-11117. https://doi.org/10.1021/ja2046292
Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders
Deng, Jinxia, Li, Lihong, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2012. "Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders." Inorganic Chemistry Communications. 21, pp. 92-95. https://doi.org/10.1016/j.inoche.2012.04.021
Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres
Yan, Xuecheng, Yu, Ranbo, Xu, Yali, Li, Li, Xu, Pengfei, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2012. "Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres." Materials Research Bulletin. 47 (9), pp. 2135-2139. https://doi.org/10.1016/j.materresbull.2012.06.013
Rapid molten salt synthesis of isotropic negative thermal expansion ScF3
Hu, Lei, Chen, Jun, Fan, Longlong, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Rapid molten salt synthesis of isotropic negative thermal expansion ScF3." Journal of the American Ceramic Society. 97 (4), pp. 1009-1011. https://doi.org/10.1111/jace.12855
Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method
Hu, Lei, Chen, Jun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method." Journal of the American Ceramic Society. 97 (5), pp. 1386-1388. https://doi.org/10.1111/jace.12932
Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range
Hu, Lei, Chen, Jun, Fan, Longlong, Ren, Yang, Rong, Yangchun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range." Journal of the American Chemical Society. 136 (39), pp. 13566-13569. https://doi.org/10.1021/ja5077487
Controlled synthesis and properties of porous Cu/CeO2 microspheres
Yao, Xiang, Yang, Xiaodan, Yu, Ranbo, Xu, Pengfei, Chen, Jun and Xing, Xianran. 2015. "Controlled synthesis and properties of porous Cu/CeO2 microspheres." Materials Research Bulletin. 61, pp. 22-25. https://doi.org/10.1016/j.materresbull.2014.09.083
Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption
Sun, Jiajia, Wang, Chengrui, Zeng, Li, Xu, Pengfei, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Jin, Quan and Yu, Ranbo. 2016. "Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption." Materials Research Bulletin. 75, pp. 110-114. https://doi.org/10.1016/j.materresbull.2015.11.035
N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures
Bao, Jinrong, Zhu, Xiaowei, Liu, Ying, Li, Wenxian and Yu, Ranbo. 2014. "N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures." Materials Letters. 124, pp. 97-100. https://doi.org/10.1016/j.matlet.2014.03.014
Microstructure construction and composition modification of CeO2 macrospheres with superior performance
Jiang, Shuaiyu, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Microstructure construction and composition modification of CeO2 macrospheres with superior performance." Inorganic Chemistry Frontiers. 3 (1), pp. 92-96. https://doi.org/10.1039/c5qi00140d
Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity
Cui, Pengzhen, Wang, Jiali, Wang, Zumin, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity." Nano Research. 9 (3), pp. 593-601. https://doi.org/10.1007/s12274-015-0939-z
A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite
Wang, Shuo, Yi, Luoxin, Halpert, Jonathan E., Lai, Xiaoyong, Liu, Yuanyuan, Cao, Hongbin, Wang, Dan, Yu, Ranbo and Li, Yuliang. 2012. "A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite." Small. 8 (2), pp. 265-271. https://doi.org/10.1002/smll.201101686
Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays
Ge, Lei, Chen, Jiuling, Chen, Jun, Zhu, Zhonghua and Rudolph, Victor. 2012. "Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays." Journal of Nanoscience and Nanotechnology. 12 (3), pp. 2722-2732. https://doi.org/10.1166/jnn.2012.5726
Research difference of strain distribution and microstructure evolution between rolling direction and transverse direction of AM50 Mg alloy plate by digital image correlation
Li, Qiang, Hua, Fuan, Li, Jianping and Wang, Hao. 2015. "Research difference of strain distribution and microstructure evolution between rolling direction and transverse direction of AM50 Mg alloy plate by digital image correlation ." Advances in Materials Science and Engineering. 2015. https://doi.org/10.1155/2015/175873
Embeddable and locatable spinning
Xu, Weilin, Xia, Zhigang, Wang, Xin, Chen, Jun, Cui, Weigang, Ye, Wenxiang, Ding, Cailing and Wang, Xungai. 2011. "Embeddable and locatable spinning." Textile Research Journal. 81 (3), pp. 223-229. https://doi.org/10.1177/0040517510380780
Durability of fly ash based-geopolymers: effect of crystallization on mechanical properties
Zhang, Zuhua, Wang, Hao, Provis, John L., Reid, Andrew and Li, Qiang. 2013. "Durability of fly ash based-geopolymers: effect of crystallization on mechanical properties." Wensheng, Zhang (ed.) 8th International Symposium on Cement and Concrete (ISCC 2013). Nanjing, China 20 - 23 Sep 2013 Beijing, China.
Numerical simulation of porosity on thermal properties and fire resistance of foamed concrete
Li, Qiang, Wang, Hao, Zhang, Zuhua and Reid, Andrew. 2013. "Numerical simulation of porosity on thermal properties and fire resistance of foamed concrete." Journal of Sustainable Cement-Based Materials. 2 (1), pp. 13-19. https://doi.org/10.1080/21650373.2012.755748
Numerical simulation of porous structure in foam concrete on thermal insulation property
Li, Qiang, Wang, Hao, Bullen, Frank and Reid, Andrew. 2012. "Numerical simulation of porous structure in foam concrete on thermal insulation property ." Jaafar, M, Azura, A. R., Leong, K. H. and Leong, A. Y. L. (ed.) 8th Asian-Australasian Conference on Composite Materials (ACCM 2012): Composites: Enabling Tomorrow's Industry Today. Kuala Lumpur, Malaysia 06 - 08 Nov 2012 Kowloon, Hong Kong.
Numerical simulation the temperature field of the multi-coil batch during annealing process in Bell-type furnace
Mo, Chun-li, Li, Qiang, Guo, Xu-ming and Wang, Hao. 2012. "Numerical simulation the temperature field of the multi-coil batch during annealing process in Bell-type furnace." 2nd International Conference on Advanced Engineering Materials and Technology (AEMT 2012). Zhuhai, China 06 Jul 2012 Zurich, Switzerland. https://doi.org/10.4028/www.scientific.net/AMR.538-541.637
Numerical simulation of rolling process and microstructure evolution of AM50 Mg alloy during hot rolling process
Hua, Fuan, Zhang, Chaoyi, Li, Qiang, Yu, Baoyi, Liu, Weihua, Li, Runxia, Xie, Shuisheng, Huang, Guojie, Cheng, Lei, Fu, Yao and Wang, Hao. 2011. "Numerical simulation of rolling process and microstructure evolution of AM50 Mg alloy during hot rolling process ." Advanced Materials Research. 291-294, pp. 449-454. https://doi.org/10.4028/www.scientific.net/AMR.291-294.449
Solidification microstructure modelling using cellular automaton method
Wang, H. and Li, Q.. 2008. "Solidification microstructure modelling using cellular automaton method." International Conference on Frontiers in Materials Science and Technology (FMST 2008). Brisbane, Australia 26 - 28 Mar 2008 Zurich, Switzerland. https://doi.org/10.4028/www.scientific.net/AMR.32.271
Cellular automaton modeling of semisolid microstructure formation
Li, Qiang, Yu, Baoyi, Zhang, Huawen, Li, Runxia, Wang, Feng, Xie, Shuisheng, Huang, Guojie and Wang, Hao. 2010. "Cellular automaton modeling of semisolid microstructure formation." China Foundry. 7 (2), pp. 143-148.
Facile one-pot synthesis of MOF supported gold pseudo-single-atom catalysts for hydrogenation reactions
Wang, Zumin, Gu, Lin, Song, Li, Wang, Hao and Yu, Ranbo. 201. "Facile one-pot synthesis of MOF supported gold pseudo-single-atom catalysts for hydrogenation reactions." Materials Chemistry Frontiers. 2 (5), pp. 1024-1030. https://doi.org/10.1039/c8qm00081f