Precursor-induced fabrication of β-Bi2O3 microspheres and their performance as visible-light-driven photocatalysts

Article

Wang, Jiali, Yang, Xiaodan, Zhao, Kun, Xu, Pengfei, Zong, Lingbo, Yu, Ranbo, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2013. "Precursor-induced fabrication of β-Bi2O3 microspheres and their performance as visible-light-driven photocatalysts ." Journal of Materials Chemistry A. 1 (32), pp. 9069-9074. https://doi.org/10.1039/c3ta11652b
Article Title

Precursor-induced fabrication of β-Bi2O3 microspheres and their performance as visible-light-driven photocatalysts

ERA Journal ID201058
Article CategoryArticle
AuthorsWang, Jiali (Author), Yang, Xiaodan (Author), Zhao, Kun (Author), Xu, Pengfei (Author), Zong, Lingbo (Author), Yu, Ranbo (Author), Wang, Dan (Author), Deng, Jinxia (Author), Chen, Jun (Author) and Xing, Xianran (Author)
Journal TitleJournal of Materials Chemistry A
Journal Citation1 (32), pp. 9069-9074
Number of Pages6
Year2013
PublisherThe Royal Society of Chemistry
Place of PublicationUnited Kingdom
ISSN2050-7488
2050-7496
Digital Object Identifier (DOI)https://doi.org/10.1039/c3ta11652b
Web Address (URL)http://pubs.rsc.org/en/Content/ArticleLanding/2013/TA/c3ta11652b#!divAbstract
Abstract

Flower-like β-Bi2O3 microspheres with high specific surface area and excellent visible-light-driven photocatalytic activity (for degradation of Rhodamine B) were successfully synthesized via a facile hydrothermal process and subsequent calcination. By precisely adjusting the hydrothermal conditions, the composition and morphology of the microspherical precursors could be well controlled, so that upon further optimized calcination of the precursors, the selective formation of the monoclinic α-Bi2O3 and tetragonal β-Bi2O3 with three dimensional (3D) hierarchical architectures could be achieved. These tetragonal β-Bi2O3 microspheres with an average diameter of 3 μm were constructed by nanoflakes with an average thickness of 50 nm, which, as far as we know, is the first reported result on the 3D hierarchical architectures of tetragonal β-Bi2O3. Its flower-like microspherical architecture made the tetragonal β-Bi2O3 possess not only much improved specific surface area but also a narrower band gap, which significantly enhanced its visible-light-driven photocatalytic activity for the degradation of Rhodamine B (RhB). To further optimize the synthetic conditions and realize the controllable synthesis, the formation mechanism for the morphologies and polymorphs of the Bi2O3 microspheres was discussed in detail.

Keywordscontrollable synthesis; hierarchical architectures; high specific surface area; hydrothermal conditions; hydrothermal process; photocatalytic activities; visible-light-driven; visible-light-driven photocatalysts; Materials Science; optimization techniques; engineering graphics; rubber and elastomers; chemical agents and basic industrial chemicals; chemical operations; chemical reactions; non mechanical properties and tests of building materials; buildings and towers
ANZSRC Field of Research 2020340399. Macromolecular and materials chemistry not elsewhere classified
340601. Catalysis and mechanisms of reactions
400408. Reaction engineering (excl. nuclear reactions)
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Byline AffiliationsUniversity of Science and Technology Beijing, China
Chinese Academy of Sciences, China
Institution of OriginUniversity of Southern Queensland
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Wang, You, Wang, Yun, Chen, Jun, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2015. "Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing." European Journal of Inorganic Chemistry. 2015 (35), pp. 5767-5772. https://doi.org/10.1002/ejic.201500869
Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries
Wang, Feng, Wang, Jiangyan, Ren, Hao, Tang, Hongjie, Yu, Ranbo and Wang, Dan. 2016. "Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries." Inorganic Chemistry Frontiers. 3 (3), pp. 365-369. https://doi.org/10.1039/c5qi00213c
Phase transformation and negative thermal expansion in TaVO5
Wang, Xiaowei, Huang, Qingzhen, Deng, Jinxia, Yu, Ranbo, Chen, Jun and Xing, Xianran. 2011. "Phase transformation and negative thermal expansion in TaVO5." Inorganic Chemistry: including bioinorganic chemistry. 50 (6), pp. 2685-2690. https://doi.org/10.1021/ic200003n
Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor
Yan, Xuecheng, Yu, Ranbo, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2011. "Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor." Solid State Sciences. 13 (5), pp. 1060-1064. https://doi.org/10.1016/j.solidstatesciences.2011.01.019
The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds
Chen, Jun, Nittala, Krishna, Forrester, Jennifer S., Jones, Jacob L., Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2011. "The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds." Journal of the American Chemical Society. 133 (29), pp. 11114-11117. https://doi.org/10.1021/ja2046292
Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders
Deng, Jinxia, Li, Lihong, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2012. "Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders." Inorganic Chemistry Communications. 21, pp. 92-95. https://doi.org/10.1016/j.inoche.2012.04.021
Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres
Yan, Xuecheng, Yu, Ranbo, Xu, Yali, Li, Li, Xu, Pengfei, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2012. "Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres." Materials Research Bulletin. 47 (9), pp. 2135-2139. https://doi.org/10.1016/j.materresbull.2012.06.013
Rapid molten salt synthesis of isotropic negative thermal expansion ScF3
Hu, Lei, Chen, Jun, Fan, Longlong, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Rapid molten salt synthesis of isotropic negative thermal expansion ScF3." Journal of the American Ceramic Society. 97 (4), pp. 1009-1011. https://doi.org/10.1111/jace.12855
Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method
Hu, Lei, Chen, Jun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method." Journal of the American Ceramic Society. 97 (5), pp. 1386-1388. https://doi.org/10.1111/jace.12932
Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range
Hu, Lei, Chen, Jun, Fan, Longlong, Ren, Yang, Rong, Yangchun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range." Journal of the American Chemical Society. 136 (39), pp. 13566-13569. https://doi.org/10.1021/ja5077487
Controlled synthesis and properties of porous Cu/CeO2 microspheres
Yao, Xiang, Yang, Xiaodan, Yu, Ranbo, Xu, Pengfei, Chen, Jun and Xing, Xianran. 2015. "Controlled synthesis and properties of porous Cu/CeO2 microspheres." Materials Research Bulletin. 61, pp. 22-25. https://doi.org/10.1016/j.materresbull.2014.09.083
Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption
Sun, Jiajia, Wang, Chengrui, Zeng, Li, Xu, Pengfei, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Jin, Quan and Yu, Ranbo. 2016. "Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption." Materials Research Bulletin. 75, pp. 110-114. https://doi.org/10.1016/j.materresbull.2015.11.035
N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures
Bao, Jinrong, Zhu, Xiaowei, Liu, Ying, Li, Wenxian and Yu, Ranbo. 2014. "N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures." Materials Letters. 124, pp. 97-100. https://doi.org/10.1016/j.matlet.2014.03.014
Microstructure construction and composition modification of CeO2 macrospheres with superior performance
Jiang, Shuaiyu, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Microstructure construction and composition modification of CeO2 macrospheres with superior performance." Inorganic Chemistry Frontiers. 3 (1), pp. 92-96. https://doi.org/10.1039/c5qi00140d
Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity
Cui, Pengzhen, Wang, Jiali, Wang, Zumin, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity." Nano Research. 9 (3), pp. 593-601. https://doi.org/10.1007/s12274-015-0939-z
A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite
Wang, Shuo, Yi, Luoxin, Halpert, Jonathan E., Lai, Xiaoyong, Liu, Yuanyuan, Cao, Hongbin, Wang, Dan, Yu, Ranbo and Li, Yuliang. 2012. "A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite." Small. 8 (2), pp. 265-271. https://doi.org/10.1002/smll.201101686
Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays
Ge, Lei, Chen, Jiuling, Chen, Jun, Zhu, Zhonghua and Rudolph, Victor. 2012. "Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays." Journal of Nanoscience and Nanotechnology. 12 (3), pp. 2722-2732. https://doi.org/10.1166/jnn.2012.5726
Elevated atmospheric [CO2] stimulates sugar accumulation and cellulose degradation rates of rice straw
Zhu, Chunwa, Xu, Xi, Wang, Dan, Zhu, Jianguo, Liu, Gang and Seneweera, Saman. 2016. "Elevated atmospheric [CO2] stimulates sugar accumulation and cellulose degradation rates of rice straw." GCB Bioenergy. 8 (3), pp. 579-587. https://doi.org/10.1111/gcbb.12277
Embeddable and locatable spinning
Xu, Weilin, Xia, Zhigang, Wang, Xin, Chen, Jun, Cui, Weigang, Ye, Wenxiang, Ding, Cailing and Wang, Xungai. 2011. "Embeddable and locatable spinning." Textile Research Journal. 81 (3), pp. 223-229. https://doi.org/10.1177/0040517510380780