Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method

Article

Hu, Lei, Chen, Jun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method." Journal of the American Ceramic Society. 97 (5), pp. 1386-1388. https://doi.org/10.1111/jace.12932
Article Title

Large-scale synthesis of isotropic single-crystalline ScF3 cubes by hydrothermal method

ERA Journal ID4948
Article CategoryArticle
AuthorsHu, Lei (Author), Chen, Jun (Author), Pan, Zhao (Author), Deng, Jinxia (Author), Yu, Ranbo (Author) and Xing, Xianran (Author)
Journal TitleJournal of the American Ceramic Society
Journal Citation97 (5), pp. 1386-1388
Number of Pages3
Year2014
Place of PublicationUnited States
ISSN0002-7820
1551-2916
Digital Object Identifier (DOI)https://doi.org/10.1111/jace.12932
Web Address (URL)http://onlinelibrary.wiley.com/doi/10.1111/jace.12932/abstract
Abstract

Scandium fluoride (ScF3) belongs to one of the rare compounds which exhibit isotropic negative thermal expansion. Here, a facile and environmentally friendly hydrothermal synthesis method has been presented. High-quality single-crystalline ScF3 cubes, with an average size of 200 nm, can be easily fabricated in a large scale. Sc(NO3) 3 and NH4HF2 were used as precursors. The as-prepared ScF3 demonstrates cubic symmetry (Pm-3 m), which was confirmed by X-ray diffraction and selected-area electron diffraction. Its uniform morphology and size were characterized by high-resolution transmission electron microscopy. Furthermore, thermal analysis was also performed in argon gas atmosphere to investigate its thermal stability.

KeywordsArgon gas atmospheres; Cubic symmetry; Hydrothermal methods; Isotropic negative thermal expansion; Large scale synthesis; Morphology and size; Selected area electron diffraction; Single-crystalline; Optical Devices and Systems; Chemistry; Chemical Reactions; Chemical Products Generally; Atomic and Molecular Physics; Nuclear Physics; Crystalline Solids;
ANZSRC Field of Research 2020401699. Materials engineering not elsewhere classified
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Byline AffiliationsUniversity of Science and Technology Beijing, China
Institution of OriginUniversity of Southern Queensland
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Hierarchical hydroxyapatite microspheres composed of nanorods and their competitive sorption behavior for heavy metal ions
Zhu, Ronghai, Lai, Xiaoyong, Halpert, Jonathan E., Yu, Ranbo and Wang, Dan. 2012. "Hierarchical hydroxyapatite microspheres composed of nanorods and their competitive sorption behavior for heavy metal ions." European Journal of Inorganic Chemistry. https://doi.org/10.1002/ejic.201101038
Water-soluble monodispersed lanthanide oxide submicrospheres: PVP-assisted hydrothermal synthesis, size-control and luminescence properties
Cui, Ying, Lai, Xiaoyong, Li, Li, Hu, Zhudong, Wang, Shuo, Halpert, Jonathan E., Yu, Ranbo and Wang, Dan. 2012. "Water-soluble monodispersed lanthanide oxide submicrospheres: PVP-assisted hydrothermal synthesis, size-control and luminescence properties." ChemPhysChem: a European journal of chemical physics and physical chemistry. 13 (10), pp. 2610-2614. https://doi.org/10.1002/cphc.201100806
One step molten salt synthesis of YVO4 nanoparticles and their photocatalytic properties under UV-Visible light
An, Xiaoxin, Wang, You, Deng, Jinxia, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2014. "One step molten salt synthesis of YVO4 nanoparticles and their photocatalytic properties under UV-Visible light." Inorganic Chemistry Communications. 44, pp. 79-82. https://doi.org/10.1016/j.inoche.2014.03.010
A low-cost and large-scale synthesis of nano-zinc oxide from smithsonite
Zhang, Yucheng, Deng, Jinxia, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2014. "A low-cost and large-scale synthesis of nano-zinc oxide from smithsonite." Inorganic Chemistry Communications. 43, pp. 138-141. https://doi.org/10.1016/j.inoche.2014.02.032
Quintuple-shelled Sno2 hollow microspheres with superior light scattering for high-performance dye-sensitized solar cells
Dong, Zhenghong, Ren, Hao, Hessel, Colin M., Wang, Jiangyan, Yu, Ranbo, Jin, Quan, Yang, Mei, Hu, Zhudong, Chen, Yunfa, Tang, Zhiyong, Zhao, Huijun and Wang, Dan. 2014. "Quintuple-shelled Sno2 hollow microspheres with superior light scattering for high-performance dye-sensitized solar cells." Advanced Materials. 26 (6), pp. 905-909. https://doi.org/10.1002/adma.201304010
Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing
Wang, You, Wang, Yun, Chen, Jun, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2015. "Nd1-xCaxFeO3 (x = 0, 0.3) hollow core-shell microspheres for ethanol gas sensing." European Journal of Inorganic Chemistry. 2015 (35), pp. 5767-5772. https://doi.org/10.1002/ejic.201500869
Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries
Wang, Feng, Wang, Jiangyan, Ren, Hao, Tang, Hongjie, Yu, Ranbo and Wang, Dan. 2016. "Multi-shelled LiMn2O4 hollow microspheres as superior cathode materials for lithium-ion batteries." Inorganic Chemistry Frontiers. 3 (3), pp. 365-369. https://doi.org/10.1039/c5qi00213c
Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor
Yan, Xuecheng, Yu, Ranbo, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2011. "Facile solvothermal synthesis of gear-shaped submicrostructured Y2O3:Eu 3+ phosphor." Solid State Sciences. 13 (5), pp. 1060-1064. https://doi.org/10.1016/j.solidstatesciences.2011.01.019
The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds
Chen, Jun, Nittala, Krishna, Forrester, Jennifer S., Jones, Jacob L., Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2011. "The role of spontaneous polarization in the negative thermal expansion of tetragonal PbTiO3-based compounds." Journal of the American Chemical Society. 133 (29), pp. 11114-11117. https://doi.org/10.1021/ja2046292
Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders
Deng, Jinxia, Li, Lihong, Chen, Jun, Yu, Ranbo and Xing, Xianran. 2012. "Facile molten salt synthesis of ordered perovskite Ba(Sr 1/3Nb 2/3)O3 powders." Inorganic Chemistry Communications. 21, pp. 92-95. https://doi.org/10.1016/j.inoche.2012.04.021
Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres
Yan, Xuecheng, Yu, Ranbo, Xu, Yali, Li, Li, Xu, Pengfei, Wang, Dan, Deng, Jinxia, Chen, Jun and Xing, Xianran. 2012. "Morphology-tailored synthesis of flower-like Y 2O 3:Eu3+ microspheres." Materials Research Bulletin. 47 (9), pp. 2135-2139. https://doi.org/10.1016/j.materresbull.2012.06.013
Rapid molten salt synthesis of isotropic negative thermal expansion ScF3
Hu, Lei, Chen, Jun, Fan, Longlong, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Rapid molten salt synthesis of isotropic negative thermal expansion ScF3." Journal of the American Ceramic Society. 97 (4), pp. 1009-1011. https://doi.org/10.1111/jace.12855
Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range
Hu, Lei, Chen, Jun, Fan, Longlong, Ren, Yang, Rong, Yangchun, Pan, Zhao, Deng, Jinxia, Yu, Ranbo and Xing, Xianran. 2014. "Zero thermal expansion and ferromagnetism in cubic sc1-xMxF3 (M = Ga, Fe) over a wide temperature range." Journal of the American Chemical Society. 136 (39), pp. 13566-13569. https://doi.org/10.1021/ja5077487
Controlled synthesis and properties of porous Cu/CeO2 microspheres
Yao, Xiang, Yang, Xiaodan, Yu, Ranbo, Xu, Pengfei, Chen, Jun and Xing, Xianran. 2015. "Controlled synthesis and properties of porous Cu/CeO2 microspheres." Materials Research Bulletin. 61, pp. 22-25. https://doi.org/10.1016/j.materresbull.2014.09.083
Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption
Sun, Jiajia, Wang, Chengrui, Zeng, Li, Xu, Pengfei, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Jin, Quan and Yu, Ranbo. 2016. "Controllable assembly of CeO2 micro/nanospheres with adjustable size and their application in Cr(VI) adsorption." Materials Research Bulletin. 75, pp. 110-114. https://doi.org/10.1016/j.materresbull.2015.11.035
N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures
Bao, Jinrong, Zhu, Xiaowei, Liu, Ying, Li, Wenxian and Yu, Ranbo. 2014. "N,N-dimethylformamide-induced synthesis and photoluminescence of CePO4 and Ce0.95PO4:Tb0.05 with sphere-like nanostructures." Materials Letters. 124, pp. 97-100. https://doi.org/10.1016/j.matlet.2014.03.014
Microstructure construction and composition modification of CeO2 macrospheres with superior performance
Jiang, Shuaiyu, Yang, Xiaodan, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Microstructure construction and composition modification of CeO2 macrospheres with superior performance." Inorganic Chemistry Frontiers. 3 (1), pp. 92-96. https://doi.org/10.1039/c5qi00140d
Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity
Cui, Pengzhen, Wang, Jiali, Wang, Zumin, Chen, Jun, Xing, Xianran, Wang, Lianzhou and Yu, Ranbo. 2016. "Bismuth oxychloride hollow microspheres with high visible light photocatalytic activity." Nano Research. 9 (3), pp. 593-601. https://doi.org/10.1007/s12274-015-0939-z
A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite
Wang, Shuo, Yi, Luoxin, Halpert, Jonathan E., Lai, Xiaoyong, Liu, Yuanyuan, Cao, Hongbin, Wang, Dan, Yu, Ranbo and Li, Yuliang. 2012. "A novel and highly efficient photocatalyst based on P 25- graphdiyne nanocomposite." Small. 8 (2), pp. 265-271. https://doi.org/10.1002/smll.201101686
Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays
Ge, Lei, Chen, Jiuling, Chen, Jun, Zhu, Zhonghua and Rudolph, Victor. 2012. "Study on the controllable scale-up growth of vertically-aligned carbon nanotube arrays." Journal of Nanoscience and Nanotechnology. 12 (3), pp. 2722-2732. https://doi.org/10.1166/jnn.2012.5726
Embeddable and locatable spinning
Xu, Weilin, Xia, Zhigang, Wang, Xin, Chen, Jun, Cui, Weigang, Ye, Wenxiang, Ding, Cailing and Wang, Xungai. 2011. "Embeddable and locatable spinning." Textile Research Journal. 81 (3), pp. 223-229. https://doi.org/10.1177/0040517510380780