Enhanced mechanical properties at 400 °C of carbon fabric reinforced phthalonitrile composites by high temperature postcure
Article
Sun, Bao-Gang, Lei, Qin, Guo, Ying, Shi, Han-Qiao, Sun, Jian-Bo, Yang, Kun-Xiao, Zhou, Heng, Li, Yuan-Qing, Hu, Ning, Wang, Hao and Fu, Shao-Yun. "Enhanced mechanical properties at 400 °C of carbon fabric reinforced phthalonitrile composites by high temperature postcure
." Composites Part B: Engineering. 166, pp. 681-687. https://doi.org/10.1016/j.compositesb.2019.02.066
| Article Title | Enhanced mechanical properties at 400 °C of carbon fabric reinforced phthalonitrile composites by high temperature postcure |
|---|---|
| ERA Journal ID | 4883 |
| Article Category | Article |
| Authors | Sun, Bao-Gang, Lei, Qin, Guo, Ying, Shi, Han-Qiao, Sun, Jian-Bo, Yang, Kun-Xiao, Zhou, Heng, Li, Yuan-Qing, Hu, Ning, Wang, Hao and Fu, Shao-Yun |
| Journal Title | Composites Part B: Engineering |
| Journal Citation | 166, pp. 681-687 |
| Number of Pages | 7 |
| Publisher | Elsevier |
| ISSN | 1359-8368 |
| Digital Object Identifier (DOI) | https://doi.org/10.1016/j.compositesb.2019.02.066 |
| Web Address (URL) | https://www.sciencedirect.com/science/article/abs/pii/S135983681833508X |
| Abstract | Phthalonitrile resins have received growing attention due to their superior thermal stability and good structural properties required for high temperature applications in aerospace industry etc. In this work, a newly developed phthalonitrile blend resin with an appropriate viscosity for autoclave processing is employed for manufacturing of high quality void-free thick composite panels using MT300 carbon fabrics. In particular, the effects of postcure temperature are systematically examined on their 400 °C mechanical properties required for high temperature structural applications. Dynamic mechanical analysis reveals that the composite postcured at the high temperature of 375 °C exhibits a high glass transition temperature over 450 °C. Mechanical testing results show that the flexural and compressive strengths at room temperature are lowered by the high temperature postcure, but their counterparts at 400 °C are obviously enhanced by the postcure. Moreover, the 400 °C interlaminar shear strength initially decreases but then increases with increasing the postcure temperature. The char retention in nitrogen at 1000 °C is 89% of its initial weight. Consequently, the newly developed phthalonitrile resin is highly promising for manufacturing of thermal resistant polymeric composites for high temperature application in aerospace industry etc. that need composites to have high temperature capabilities. |
| Keywords | carbon fiber reinforced composite; phthalonitrile; elevated temperature; mechanical properties; postcure |
| Contains Sensitive Content | Does not contain sensitive content |
| ANZSRC Field of Research 2020 | 401602. Composite and hybrid materials |
| Public Notes | Files associated with this item cannot be displayed due to copyright restrictions. |
| Byline Affiliations | Chongqing University, China |
| Aerospace Research Institute of Materials & Processing Technology, China | |
| Chinese Academy of Sciences, China | |
| Centre for Future Materials |
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Wang, Yuan, Liu, Wei-Di, Shi, XIao-Lei, Hong, Min, Wang, Li-Jun, Li, Meng, Wang, Hao, Zou, Jin and Chen, Zhi-Gang. 2020. "Enhanced thermoelectric properties of nanostructured n-type Bi2Te3 by suppressing Te vacancy through non-equilibrium fast reaction." Chemical Engineering Journal. 391. https://doi.org/10.1016/j.cej.2019.123513Development of a new calcium sulfoaluminate (synthetic ye'elimite) blended PII 52.5 cement
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Ma, Y., Yang, X., Hu, J., Zhang, Z. and Wang, H.. 2019. "Accurate determination of the 'time-zero' of autogenous shrinkage in alkali-activated fly ash/slag system." Composites Part B: Engineering. 177, pp. 1-8. https://doi.org/10.1016/j.compositesb.2019.107367Microstructure and wear characteristics of ATZ ceramic particle reinforced gray iron matrix surface composites
Ma, Xue, Li, Liang-feng, Zhang, Fan, Zhang, Zu-hua, Wang, Hao and Wang, En-ze. 2018. "Microstructure and wear characteristics of ATZ ceramic particle reinforced gray iron matrix surface composites." China Foundry. 15 (3), pp. 167-172. https://doi.org/10.1007/s41230-018-7211-6New selective dissolution process to quantify reaction extent and product stability in metakaolin-based geopolymers
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Longhi, Marlon, Zhang, Zuhua, Rodriguez, Erich, Kirchheim, Ana and Wang, Hao. 2019. "Efflorescence of alkali-activated cements (geopolymers) and the impacts on material structures: A critical analysis." Frontiers in Materials. 6, pp. 1-13. https://doi.org/10.3389/fmats.2019.00089A review on mixture design methods for geopolymer concrete
Li, Ning, Shi, Caijun, Zhang, Zuhua, Wang, Hao and Liu, Yiwei. 2019. "A review on mixture design methods for geopolymer concrete." Composites Part B: Engineering. 178, pp. 1-14. https://doi.org/10.1016/j.compositesb.2019.107490New Insights into the Degradation Behavior of Air Electrodes during Solid Oxide Electrolysis and Reversible Solid Oxide Cell Operation
Khan, Muhammad Shirjeel, Xu, Xiaoyong, Knibbe, Ruth, Rehman, Ateeq Ur, Li, Zhiheng, Yago, Anya Josefa, Wang, Hao and Zhu, Zhonghua. 2020. "New Insights into the Degradation Behavior of Air Electrodes during Solid Oxide Electrolysis and Reversible Solid Oxide Cell Operation ." Energy Technology: generation, conversion, storage, distribution. 8 (9). https://doi.org/10.1002/ente.202000241Water absorption and chloride diffusivity of concrete under the coupling effect of uniaxial compressive load and freeze-thaw cycles
Wang, Yanru, Cao, Yubin, Zhang, Peng, Ma, Yuwei, Zhao, Tiejun, Wang, Hao and Zhang, Zuhua. 2019. "Water absorption and chloride diffusivity of concrete under the coupling effect of uniaxial compressive load and freeze-thaw cycles." Construction and Building Materials. 209, pp. 566-576. https://doi.org/10.1016/j.conbuildmat.2019.03.091High Porosity in Nanostructured n-Type Bi2Te3 Obtaining Ultralow Lattice Thermal Conductivity
Wang, Yuan, Liu, Wei-Di, Gao, Han, Wang, Li-Jun, Li, Meng, Shi, Xiao-Lei, Hong, Min, Wang, Hao, Zou, Jin and Chen, Zhi-Gang. 2019. "High Porosity in Nanostructured n-Type Bi2Te3 Obtaining Ultralow Lattice Thermal Conductivity ." ACS Applied Materials and Interfaces. 11 (34), pp. 31237-31244. https://doi.org/10.1021/acsami.9b12079Effect of drying procedures on pore structure and phase evolution of alkali-activated cements
Zhang, Zuhua, Zhu, Yingcan, Zhu, Huajun, Zhang, Yu, Provis, John L. and Wang, Hao. 2019. "Effect of drying procedures on pore structure and phase evolution of alkali-activated cements." Cement and Concrete Composites. 96, pp. 194-203. https://doi.org/10.1016/j.cemconcomp.2018.12.003Fire-resistant, strong and green polymer nanocomposites based on poly(lactic acid) and core-shell nanofibrous flame retardants
Feng, Jiabin, Sun, Yiqi, Song, Pingan, Lei, Weiwei, Wu, Qiang, Liu, Lina, Yu, Youming and Wang, Hao. 2017. "Fire-resistant, strong and green polymer nanocomposites based on poly(lactic acid) and core-shell nanofibrous flame retardants." ACS Sustainable Chemistry and Engineering. 5 (9), pp. 7894-7904. https://doi.org/10.1021/acssuschemeng.7b01430Orientated growth of copper-based MOF for acetylene storage
Wang, Zhanke, Ge, Lei, Li, Mengran, Lin, Rijia, Wang, Hao and Zhu, Zhonghua. 2019. "Orientated growth of copper-based MOF for acetylene storage." Chemical Engineering Journal. 357, pp. 320-327. https://doi.org/10.1016/j.cej.2018.09.148Bioinspired design of strong, tough, and thermally stable polymeric materials via nanoconfinement
Song, Pingan, Dai, Jinfeng, Chen, Guorong, Yu, Youming, Fang, Zhengping, Lei, Weiwei, Fu, Shenyuan, Wang, Hao and Chen, Zhi-Gang. 2018. "Bioinspired design of strong, tough, and thermally stable polymeric materials via nanoconfinement." ACS Nano. 12 (9), pp. 9266-9278. https://doi.org/10.1021/acsnano.8b04002Fabrication of flame retardant benzoxazine semi-biocomposites reinforced by ramie fabrics with bio-based flame retardant coating
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Hong, Min, Wang, Yuan, Liu, Weidi, Matsumura, Syo, Wang, Hao, Zou, Jin and Chen, Zhi-Gang. 2018. "Arrays of planar vacancies in superior thermoelectric Ge1−x−yCdxBiyTe with band convergence." Advanced Energy Materials. 8 (30), pp. 1-10. https://doi.org/10.1002/aenm.201801837Realizing zT of 2.3 in Ge1−x−ySbxInyTe via Reducing the Phase-Transition Temperature and Introducing Resonant Energy Doping
Hong, Min, Chen, Zhi-Gang, Yang, Lei, Zou, Yi-Chao, Dargusch, Matthew, Wang, Hao and Zou, Jin. 2018. "Realizing zT of 2.3 in Ge1−x−ySbxInyTe via Reducing the Phase-Transition Temperature and Introducing Resonant Energy Doping." Advanced Materials. 30 (11), pp. 1-8. https://doi.org/10.1002/adma.201705942Comparative Study on the drying shrinkage and mechanical properties of geopolymer foam concrete incorporating different dosages of fiber, sand and foam agents
Abdollahnejad, Zahra, Zhang, Zuhua, Wang, Hao and Mastali, Mohammad. 2018. "Comparative Study on the drying shrinkage and mechanical properties of geopolymer foam concrete incorporating different dosages of fiber, sand and foam agents." Hordijk, D. A. and Lukovic, M. (ed.) 2017 fib Symposium: High Tech Concrete: Where Technology and Engineering Meet. Maastricht, The Netherlands 12 - 14 Jun 2017 Cham, Switzerland.A facile way to prepare phosphorus-Nitrogen-Functionalized graphene oxide for enhancing the flame retardancy of epoxy resin
Fang, Fang, Song, Pingan, Ran, Shiya, Guo, Zhenghong, Wang, Hao and Fang, Zhenping. 2018. "A facile way to prepare phosphorus-Nitrogen-Functionalized graphene oxide for enhancing the flame retardancy of epoxy resin." Composites Communications. 10, pp. 97-102. https://doi.org/10.1016/j.coco.2018.08.001Efflorescence and subflorescence induced microstructural and mechanical evolution in fly ash-based geopolymers
Zhang, Zuhua, Provis, John L., Reid, Andrew and Wang, Hao. 2018. "Efflorescence and subflorescence induced microstructural and mechanical evolution in fly ash-based geopolymers." Cement and Concrete Composites. 92, pp. 165-177. https://doi.org/10.1016/j.cemconcomp.2018.06.010Effect of welan gum on the hydration and hardening of Portland cement
Zhang, Yu, Zhang, Zuhua, Li, Xuerun, Li, Weifeng, Shen, Xiaodong and Wang, Hao. 2018. "Effect of welan gum on the hydration and hardening of Portland cement." Journal of Thermal Analysis and Calorimetry: an international forum for thermal studies. 131 (2), pp. 1277-1286. https://doi.org/10.1007/s10973-017-6589-5Sandwich assemblies of composites square hollow sections and thin-walled panels in compression
Xie, Lei, Qi, Yujun, Bai, Yu, Qui, Chengyu, Wang Hao, Fang, Hai and Zhao, Xiao-Ling. 2019. "Sandwich assemblies of composites square hollow sections and thin-walled panels in compression ." Thin-Walled Structures. 145. https://doi.org/10.1016/j.tws.2019.106412Multiscale modeling for high-performance concrete: a review
Wu, Linmei, Liu, Peng, Zhang, Zuhua, Zhu, DeJu and Wang, Hao. 2018. "Multiscale modeling for high-performance concrete: a review ." International Journal for Multiscale Computational Engineering. 16 (1), pp. 1-17. https://doi.org/10.1615/IntJMultCompEng.2018022827A review of extending performance of epoxy resins using carbon nanomaterials
Liu, Shan, Chevali, Venkata S., Xu, Zhiguang, Hui, David and Wang, Hao. 2018. "A review of extending performance of epoxy resins using carbon nanomaterials." Composites Part B: Engineering. 136 (1), pp. 197-214. https://doi.org/10.1016/j.compositesb.2017.08.020Granular nanostructure: a facile biomimetic strategy for the design of supertough polymeric materials with high ductility and strength
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Sun, Yiqi, Sun, Shuai, Chen, Lei, Liu, Lina, Song, Pingan, Li, Wei, Yu, Youming, Lu, Fengzhu, Qian, Jun and Wang, Hao. 2017. "Flame retardant and mechanically tough poly(lactic acid) biocomposites via combining ammonia polyphosphate and polyethylene glycol." Composites Communications. 6. https://doi.org/10.1016/j.coco.2017.07.005Super-tough artificial nacre based on graphene oxide via synergistic interface interactions of Pi-Pi stacking and hydrogen bonding
Song, Pingan, Xu, Zhiguang, Wu, Yuanpeng, Cheng, Qunfeng, Guo, Qipeng and Wang, Hao. 2017. "Super-tough artificial nacre based on graphene oxide via synergistic interface interactions of Pi-Pi stacking and hydrogen bonding." Carbon. 111, pp. 807-812. https://doi.org/10.1016/j.carbon.2016.10.0672D-alumina platelets enhance mechanical and abrasion properties of PA-612 via interfacial hydrogen-bond interactions
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Fu, H. M., Qiu, D., Zhang, M. X., Wang, H., Kelly, P. M. and Taylor, J. A.. 2008. "The development of a new grain refiner for magnesium alloys using the edge-to-edge model." Journal of Alloys and Compounds. 456 (1-2), pp. 390-394. https://doi.org/10.1016/j.jallcom.2007.02.076Cu-based bulk amorphous alloy with larger glass-forming ability and supercooled liquid region
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Yao, X. D., Wu, C. Z., Wang, Hao, Cheng, H. M. and Lu, G. Q.. 2006. "Effects of Carbon Nanotubes and Metal Catalysts on Hydrogen Storage in Magnesium Nanocomposites." Journal of Nanoscience and Nanotechnology. 6 (2), pp. 494-498. https://doi.org/10.1166/jnn.2006.098In situ TiB-reinforced cu-based bulk metallic glass composites
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "In situ TiB-reinforced cu-based bulk metallic glass composites." Scripta Materialia. 54 (11), pp. 1961-1966. https://doi.org/10.1016/j.scriptamat.2006.01.048Numerical simulation of dendrite growth during solidification
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Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2006. "In-situ Cu-based bulk metallic glass composite." International Journal of Modern Physics B. 20 (25-27), pp. 3963-3968. https://doi.org/10.1142/S0217979206040696The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy." Scripta Materialia. 55 (2), pp. 147-150. https://doi.org/10.1016/j.scriptamat.2006.03.052Modeling of semisolid structure formation in controlled nucleation method
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Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "Tungsten fibre reinforced Zr-based bulk metallic glass composites ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2007. "Tungsten fibre reinforced Zr-based bulk metallic glass composites." Materials and Manufacturing Processes. 22 (5-6), pp. 687-691. https://doi.org/10.1080/10426910701384922Semisolid structure simulation in controlled nucleation process
Wang, H. and Yao, X. D.. 2006. "Semisolid structure simulation in controlled nucleation process." Solid State Phenomena. 116-117, pp. 614-617. https://doi.org/10.4028/www.scientific.net/SSP.116-117.614The effect of initial microstructure of A356 alloys on the mechanical behavior in the semisolid state
Ning, Zhiliang, Wang, Hao and Sun, Jianfei. 2006. "The effect of initial microstructure of A356 alloys on the mechanical behavior in the semisolid state." Solid State Phenomena. 116-117, pp. 449-452. https://doi.org/10.4028/www.scientific.net/SSP.116-117.449Semisolid casting of automotive component: water pump lid
Wang, Hao and Xu, Jun. 2006. "Semisolid casting of automotive component: water pump lid." Solid State Phenomena. 116-117, pp. 88-91. https://doi.org/10.4028/www.scientific.net/SSP.116-117.88The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ
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Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao and Canning, John. 2010. "Effects of the self distortions of embedded FBG sensors on spectral response due to torsional and combined loads." 3rd Asia-Pacific Workshop on Structural Health Monitoring (APWSHM 2010). Tokyo, Japan 30 Nov - 02 Dec 2010 Tokyo, Japan.Natural fibre composites with epoxidized vegetable oil (EVO) resins: a review
Manthey, N. W., Cardona, F., Aravinthan, T., Wang, H. and Cooney, T.. 2010. "Natural fibre composites with epoxidized vegetable oil (EVO) resins: a review." Goh, Steven C. and Wang, Hao (ed.) 2010 Southern Region Engineering Conference (SREC 2010). Toowoomba, Australia 11 - 12 Nov 2010 Toowoomba, Australia.Magnesium and magnesium alloys as degradable metallic biomaterials
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Ning, Zhiliang, Wu, Peilian, Wang, Hao, Cao, Fuyang and Sun, Jianfei. 2007. "Effect of pouring temperature on thixotropic microstructure formation of AZ91." Rare Metals. 26 (S1), pp. 180-184.Anomalous grain coarsening behaviour observed in grain-refined aluminium alloy cast using low superheat
Taylor, J. A., Wang, H., StJohn, D. H. and Bainbridge, I. F.. 2001. "Anomalous grain coarsening behaviour observed in grain-refined aluminium alloy cast using low superheat." Anjier, Joseph L. (ed.) 130th TMS Annual MeetingLight Metals 2001. New Orleans, Louisanna 11 - 15 Feb 2001 Warrendale, PA. United States.Semisolid microstructural evolution of AlSi7Mg during partial remelting
Wang, Hao, Davidson, C. J. and StJohn, David H.. 2004. "Semisolid microstructural evolution of AlSi7Mg during partial remelting." Materials Science and Engineering A: Structural Materials: Properties, Microstructure and Processing. 368 (1-2), pp. 159-167. https://doi.org/10.1016/j.msea.2003.10.305Biocorrosion behaviour of magnesium alloys under pseudo-physiological conditions
Wang, Hao, Zhang, M. X., Shi, Z. M. and Yang, Ke. 2006. "Biocorrosion behaviour of magnesium alloys under pseudo-physiological conditions." Tissue Engineering. 12 (4), pp. 1067-1067.Facile one-pot synthesis of MOF supported gold pseudo-single-atom catalysts for hydrogenation reactions
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