Green and Facile Synthesis of Bio-Based, Flame-Retardant, Latent Imidazole Curing Agent for Single-Component Epoxy Resin
Article
Wang, Jingsheng, Huo, Siqi, Wang, Jun, Yang, Shuang, Chen, Kaiwen, Li, Chang, Fang, De, Fang, Zhengping, Song, Pingan and Wang, Hao. 2022. "Green and Facile Synthesis of Bio-Based, Flame-Retardant, Latent Imidazole Curing Agent for Single-Component Epoxy Resin
." ACS Applied Polymer Materials. 4 (5), pp. 3564-3574. https://doi.org/10.1021/acsapm.2c00138
| Article Title | Green and Facile Synthesis of Bio-Based, Flame-Retardant, Latent Imidazole Curing Agent for Single-Component Epoxy Resin |
|---|---|
| ERA Journal ID | 211585 |
| Article Category | Article |
| Authors | Wang, Jingsheng, Huo, Siqi, Wang, Jun, Yang, Shuang, Chen, Kaiwen, Li, Chang, Fang, De, Fang, Zhengping, Song, Pingan and Wang, Hao |
| Journal Title | ACS Applied Polymer Materials |
| Journal Citation | 4 (5), pp. 3564-3574 |
| Number of Pages | 11 |
| Year | 2022 |
| Publisher | American Chemical Society |
| Place of Publication | United States |
| ISSN | 2637-6105 |
| Digital Object Identifier (DOI) | https://doi.org/10.1021/acsapm.2c00138 |
| Web Address (URL) | https://pubs.acs.org/doi/10.1021/acsapm.2c00138 |
| Abstract | Developing bio-based flame retardants according to a green and simple strategy has drawn extensive attention recently. Hence, a biomass-derived, flame-retardant, latent curing agent (IMPA) was synthesized via the neutralization between imidazole and phytic acid in water at room temperature and was applied for single-component epoxy resin (EP). The results indicate that the shelf life of the resultant EP (EP/IMPA) increases from <1 day of the control single-component EP to 10 days at room temperature. Meanwhile, EP/IMPA features a fast curing rate at modest temperature (80–150 °C), and its gel time at 100 °C is only 14 min. Notably, EP/IMPA achieves superior flame retardancy with a limiting oxygen index of 34.7% and UL-94 V-0 rating. The peak heat release rate (PHRR), total heat release (THR), and total smoke production (TSP) of EP/IMPA are reduced by 43.0%, 31.9%, and 31.5% compared with the control sample. The enhanced fire safety is ascribed to the flame-retardant function of IMPA in both gaseous and condensed phases. Hence, this work provides a green and feasible method to create bio-based, flame-retardant, latent curing agents for one-component epoxy systems. |
| Keywords | epoxy resin; bio-based latent curing agent; curing behaviors; storage stability; flame retardancy; smoke suppression |
| ANZSRC Field of Research 2020 | 401609. Polymers and plastics |
| Public Notes | Files associated with this item cannot be displayed due to copyright restrictions. |
| Byline Affiliations | Wuhan University of Technology, China |
| School of Engineering | |
| Imperial College London, United Kingdom | |
| NingboTech University, China | |
| Zhejiang University, China | |
| Centre for Future Materials | |
| School of Agriculture and Environmental Science |
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Guo, Kun-Yu, Wu, Qian, Mao, Min, Chen, Heng, Zhang, Guo-Dong, Zhao, Li, Gao, Jie-Feng, Song, Pingan and Tang, Long-Cheng. 2020. "Water-based hybrid coatings toward mechanically flexible, super-hydrophobic and flame-retardant polyurethane foam nanocomposites with high-efficiency and reliable fire alarm response." Composites Part B: Engineering. 193, pp. 1-11. https://doi.org/10.1016/j.compositesb.2020.108017One-step and green synthesis of lightweight, mechanically flexible and flame-retardant polydimethylsiloxane foam nanocomposites via surface-assembling ultralow content of graphene derivative
Cao, Cheng-Fei, Wang, Peng-Huan, Zhang, Jian-Wang, Guo, Kun-Yu, Li, Yan, Xia, Qiao-Qi, Zhang, Guo-Dong, Zhao, Li, Chen, Heng, Wang, Luobin, Gao, Jie-Feng, Song, Pingan and Tang, Long-Cheng. 2020. "One-step and green synthesis of lightweight, mechanically flexible and flame-retardant polydimethylsiloxane foam nanocomposites via surface-assembling ultralow content of graphene derivative." Chemical Engineering Journal. 393, pp. 1-13. https://doi.org/10.1016/j.cej.2020.124724Highly Flexible Multilayered e-Skins for Thermal-Magnetic-Mechanical Triple Sensors and Intelligent Grippers
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Xu, Xiaodong, Dai, Jinfeng, Ma, Zhewen, Liu, Lina, Zhang, Xinghong, Liu, Hongzhi, Tang, Long-Cheng, Huang, Guobo, Wang, Hao and Song, Pingan. 2020. "Manipulating interphase reactions for mechanically robust, flame-retardant and sustainable polylactide biocomposites." Composites Part B: Engineering. 190, pp. 1-15. https://doi.org/10.1016/j.compositesb.2020.107930Grafting Lignin with Bioderived Polyacrylates for Low-Cost, Ductile, and Fully Biobased Poly(lactic acid) Composite
Sun, Yiqi, Ma, Zhewen, Xu, Xiaodong, Liu, Xiaohuan, Liu, Lina, Huang, Guobo, Liu, Lei, Wang, Hao and Song, Pingan. 2020. "Grafting Lignin with Bioderived Polyacrylates for Low-Cost, Ductile, and Fully Biobased Poly(lactic acid) Composite." ACS Sustainable Chemistry and Engineering. 8 (5), pp. 2267-2276. https://doi.org/10.1021/acssuschemeng.9b06593A liquid phosphorus-containing imidazole derivative as flame-retardant curing agent for epoxy resin with enhanced thermal latency, mechanical, and flame-retardant performances
Huo, Siqi, Yang, Shuang, Wang, Jun, Cheng, Jianwen, Zhang, Qianqian, Hu, Yefa, Ding, Guoping, Zhang, Qiaoxin and Song, Pingan. 2020. "A liquid phosphorus-containing imidazole derivative as flame-retardant curing agent for epoxy resin with enhanced thermal latency, mechanical, and flame-retardant performances." Journal of Hazardous Materials. 386, pp. 1-10. https://doi.org/10.1016/j.jhazmat.2019.121984A novel strategy for enhancing the flame resistance, dynamic mechanical and the thermal degradation properties of epoxy nanocomposites
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Yu, Zhi-Ran, Li, Shi-Neng, Zang, Jing, Zhang, Ming, Gong, Li-Xiu, Song, Pingan, Zhao, Li, Zhang, Guo-Dong and Tang, Long-Cheng. 2019. "Enhanced mechanical property and flame resistance of graphene oxide nanocomposite paper modified with functionalized silica nanoparticles." Composites Part B: Engineering. 177, pp. 1-9. https://doi.org/10.1016/j.compositesb.2019.107347Strengthening, toughing and thermally stable ultra-thin MXene nanosheets/polypropylene nanocomposites via nanoconfinement
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Wang, Jieming, Liu, Dan, Li, Quanxiang, Chen, Cheng, Chen, Zhiqiang, Song, Pingan, Hao, Jian, Li, Yingwei, Fakhrhoseini, Sobhan, Naebe, Minoo, Wang, Xungai and Lei, Weiwei. 2019. "Lightweight, Superelastic Yet Thermoconductive Boron Nitride Nanocomposite Aerogel for Thermal Energy Regulation." ACS Nano. 13 (7), pp. 7860-7870. https://doi.org/10.1021/acsnano.9b02182A facile method to improve thermal stability and flame retardancy of polyamide 6
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Wang, Cheng, Huo, Siqi, Liu, Shi, Hu, Qinghua, Zhang, Qi and Liu, Zhitian. 2021. "Recycle of magnesium alloy scrap for improving fire resistance, thermal stability, and water tolerance of intumescent fire-retardant coatings." Journal of Coatings Technology and Research. 18 (2), pp. 447-458. https://doi.org/10.1007/s11998-020-00413-5A Novel Synergistic Flame Retardant of Hexaphenoxycyclotriphosphazene for Epoxy Resin
Jiang, Jiawei, Huo, Siqi, Zheng, Yi, Yang, Chengyun, Yan, Hongqiang, Ran, Shiya and Fang, Zhengping. 2021. "A Novel Synergistic Flame Retardant of Hexaphenoxycyclotriphosphazene for Epoxy Resin." Polymers. 13 (21), pp. 1-15. https://doi.org/10.3390/polym13213648Fabrication and Mechanism Study of Cerium-Based P, N-Containing Complexes for Reducing Fire Hazards of Polycarbonate with Superior Thermostability and Toughness
Sai, Ting, Su, Yukai, Shen, Haifeng, Ran, Shiya, Huo, Siqi, Guo, Zhenghong and Fang, Zhengping. 2021. "Fabrication and Mechanism Study of Cerium-Based P, N-Containing Complexes for Reducing Fire Hazards of Polycarbonate with Superior Thermostability and Toughness." ACS Applied Materials and Interfaces. 13 (25), pp. 30061-30075. https://doi.org/10.1021/acsami.1c07153Exfoliated and functionalized boron nitride nanosheets towards improved fire resistance and water tolerance of intumescent fire retardant coating
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Xiao, Xianglian, Chevali, Venkata S., Song, Pingan, Yu, Bin, Yang, Yihu and Wang, Hao. 2020. "Enhanced toughness of PLLA/PCL blends using poly(d-lactide)-poly(ε-caprolactone)-poly(d-lactide) as compatibilizer." Composites Communications. 21, pp. 1-6. https://doi.org/10.1016/j.coco.2020.100385Bacteria-triggered pH-responsive osteopotentiating coating on 3D-printed polyetheretherketone scaffolds for infective bone defect repair
Deng, Yi, Shi, Xiuyuan, Chen, Yong, Yang, Weizhong, Ma, Yuan, Shi, Xiao-Lei, Song, Pingan, Dargusch, Matthew S. and Chen, Zhi-Gang. 2020. "Bacteria-triggered pH-responsive osteopotentiating coating on 3D-printed polyetheretherketone scaffolds for infective bone defect repair." Industrial and Engineering Chemistry Research. 59 (26), pp. 12123-12135. https://doi.org/10.1021/acs.iecr.0c02107Direct evidence of boosted oxygen evolution over perovskite by enhanced lattice oxygen participation
Pan, Yangli, Xu, Xiaomin, Zhong, Yijun, Ge, Lei, Chen, Yubo, Veder, Jean-Pierre Marcel, Guan, Daqin, O’Hayre, Ryan, Li, Mengran, Wang, Guoxiong, Wang, Hao, Zhou, Wei and Shao, Zongping. 2020. "Direct evidence of boosted oxygen evolution over perovskite by enhanced lattice oxygen participation." Nature Communications. 11, pp. 1-10. https://doi.org/10.1038/s41467-020-15873-xCurrent status of carbon fibre and carbon fibre composites recycling
Zhang, Jin, Chevali, Venkata S., Wang, Hao and Wang, Chun-Hui. 2020. "Current status of carbon fibre and carbon fibre composites recycling." Composites Part B: Engineering. 193, pp. 1-15. https://doi.org/10.1016/j.compositesb.2020.108053Enhanced thermoelectric properties of nanostructured n-type Bi2Te3 by suppressing Te vacancy through non-equilibrium fast reaction
Wang, Yuan, Liu, Wei-Di, Shi, XIao-Lei, Hong, Min, Wang, Li-Jun, Li, Meng, Wang, Hao, Zou, Jin and Chen, Zhi-Gang. 2020. "Enhanced thermoelectric properties of nanostructured n-type Bi2Te3 by suppressing Te vacancy through non-equilibrium fast reaction." Chemical Engineering Journal. 391. https://doi.org/10.1016/j.cej.2019.123513Development of a new calcium sulfoaluminate (synthetic ye'elimite) blended PII 52.5 cement
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Ma, Y., Yang, X., Hu, J., Zhang, Z. and Wang, H.. 2019. "Accurate determination of the 'time-zero' of autogenous shrinkage in alkali-activated fly ash/slag system." Composites Part B: Engineering. 177, pp. 1-8. https://doi.org/10.1016/j.compositesb.2019.107367Microstructure and wear characteristics of ATZ ceramic particle reinforced gray iron matrix surface composites
Ma, Xue, Li, Liang-feng, Zhang, Fan, Zhang, Zu-hua, Wang, Hao and Wang, En-ze. 2018. "Microstructure and wear characteristics of ATZ ceramic particle reinforced gray iron matrix surface composites." China Foundry. 15 (3), pp. 167-172. https://doi.org/10.1007/s41230-018-7211-6New selective dissolution process to quantify reaction extent and product stability in metakaolin-based geopolymers
Longhi, Marlon, Walkley, Brant, Rodriguez, Erich D, Kirchheim, Ana P, Zhang, Zuhua and Wang, Hao. 2019. "New selective dissolution process to quantify reaction extent and product stability in metakaolin-based geopolymers." Composites Part B: Engineering. 176 (1). https://doi.org/10.1016/j.compositesb.2019.107172Polylactide/hemp hurd biocomposites as sustainable 3D printing feedstock
Xiao, Xianglian, Chevali, Venkata S., Song, Pingan, He, Dongning and Wang, Hao. 2019. "Polylactide/hemp hurd biocomposites as sustainable 3D printing feedstock." Composites Science and Technology. 184, pp. 1-8. https://doi.org/10.1016/j.compscitech.2019.107887Efflorescence of alkali-activated cements (geopolymers) and the impacts on material structures: A critical analysis
Longhi, Marlon, Zhang, Zuhua, Rodriguez, Erich, Kirchheim, Ana and Wang, Hao. 2019. "Efflorescence of alkali-activated cements (geopolymers) and the impacts on material structures: A critical analysis." Frontiers in Materials. 6, pp. 1-13. https://doi.org/10.3389/fmats.2019.00089A review on mixture design methods for geopolymer concrete
Li, Ning, Shi, Caijun, Zhang, Zuhua, Wang, Hao and Liu, Yiwei. 2019. "A review on mixture design methods for geopolymer concrete." Composites Part B: Engineering. 178, pp. 1-14. https://doi.org/10.1016/j.compositesb.2019.107490New Insights into the Degradation Behavior of Air Electrodes during Solid Oxide Electrolysis and Reversible Solid Oxide Cell Operation
Khan, Muhammad Shirjeel, Xu, Xiaoyong, Knibbe, Ruth, Rehman, Ateeq Ur, Li, Zhiheng, Yago, Anya Josefa, Wang, Hao and Zhu, Zhonghua. 2020. "New Insights into the Degradation Behavior of Air Electrodes during Solid Oxide Electrolysis and Reversible Solid Oxide Cell Operation ." Energy Technology: generation, conversion, storage, distribution. 8 (9). https://doi.org/10.1002/ente.202000241Thermal properties and flame retardancy of an intumescent flame-retarded epoxy system containing phosphaphenanthrene, triazine-trione and piperidine
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Su, Xiaogang, Wang, Jun, Zhang, Xiaoxiao, Huo, Siqi, Dai, Wei and Zhang, Bin. 2020. "Synergistic effect of polyhedral iron-cobalt alloys and graphite nanosheets with excellent microwave absorption performance." Journal of Alloys and Compounds. 829. https://doi.org/10.1016/j.jallcom.2020.154426Study on the plastic deformation zone of Q235 steel via hammering tight seam
Wang, Yingwei, Dong, Xin, Huo, Siqi, Lv, Zhenhua, Ma, Zhongnan, Gao, Jinzhu, Gai, Xiuying and Wang, Rui. 2020. "Study on the plastic deformation zone of Q235 steel via hammering tight seam." Journal of Materials Research and Technology. 9 (4), pp. 7100-7103. https://doi.org/10.1016/j.jmrt.2020.04.030A P/N-containing flame retardant constructed by phosphaphenanthrene, phosphonate, and triazole and its flame retardant mechanism in reducing fire hazards of epoxy resin
Cheng, Jianwen, Duan, Huajun, Yang, Shuang, Wang, Jun, Zhang, Qianqian, Ding, Guoping, Hu, Yefa and Huo, Siqi. 2020. "A P/N-containing flame retardant constructed by phosphaphenanthrene, phosphonate, and triazole and its flame retardant mechanism in reducing fire hazards of epoxy resin." Journal of Applied Polymer Science. 137 (37). https://doi.org/10.1002/app.49090One-step preparation of CoFe2O4/FeCo/graphite nanosheets hybrid composites with tunable microwave absorption performance
Su, Xiaogang, Wang, Jun, Zhang, Xiaoxiao, Huo, Siqi, Chen, Wei, Dai, Wei and Zhang, Bin. 2020. "One-step preparation of CoFe2O4/FeCo/graphite nanosheets hybrid composites with tunable microwave absorption performance." Ceramics International. 46 (8), pp. 12353-12363. https://doi.org/10.1016/j.ceramint.2020.01.286Intumescent fire retardant coating with recycled powder from industrial effluent optimized using response surface methodology
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Wu, Qilei, Jin, Huihui, Zhang, Bin, Huo, Siqi, Yang, Shuang, Su, Xiaogang and Wang, Jun. 2020. "Facile synthesis of cobalt-doped porous composites with amorphous carbon/zn shell for high-performance microwave absorption." Nanomaterials. 10 (2). https://doi.org/10.3390/nano10020330Facile synthesis of Co-embedded porous spherical carbon composites derived from Co3O4/ZIF-8 compounds for broadband microwave absorption
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Wang, H., Estrin, Y., Fu, H. M., Song, G. L. and Zuberova, Z.. 2007. "The effect of pre-processing and grain structure on the bio-corrosion and fatigue resistance of magnesium alloy AZ31." Advanced Engineering Materials. 9 (11), pp. 967-972. https://doi.org/10.1002/adem.200700200Bulk metallic glass composites
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