Flame-retardant, transparent, mechanically-strong and tough epoxy resin enabled by high-efficiency multifunctional boron-based polyphosphonamide
Article
Huo, Siqi, Zhou, Zhongxiao, Jiang, Jiawei, Sai, Ting, Ran, Shiya, Fang, Zhengping, Song, Pingan and Wang, Hao. 2022. "Flame-retardant, transparent, mechanically-strong and tough epoxy resin enabled by high-efficiency multifunctional boron-based polyphosphonamide." Chemical Engineering Journal. 427, pp. 1-15. https://doi.org/10.1016/j.cej.2021.131578
| Article Title | Flame-retardant, transparent, mechanically-strong and tough epoxy resin enabled by high-efficiency multifunctional boron-based polyphosphonamide |
|---|---|
| ERA Journal ID | 3854 |
| Article Category | Article |
| Authors | Huo, Siqi (Author), Zhou, Zhongxiao (Author), Jiang, Jiawei (Author), Sai, Ting (Author), Ran, Shiya (Author), Fang, Zhengping (Author), Song, Pingan (Author) and Wang, Hao (Author) |
| Journal Title | Chemical Engineering Journal |
| Journal Citation | 427, pp. 1-15 |
| Article Number | 131578 |
| Number of Pages | 15 |
| Year | 2022 |
| Publisher | Elsevier |
| Place of Publication | Netherlands |
| ISSN | 1385-8947 |
| 1873-3212 | |
| Digital Object Identifier (DOI) | https://doi.org/10.1016/j.cej.2021.131578 |
| Web Address (URL) | https://www.sciencedirect.com/science/article/pii/S1385894721031594 |
| Abstract | It is of great significance to develop high-performance epoxy resins (EPs) combining superior flame retardancy, smoke suppression, thermal oxidation stability, transparency and mechanical properties. However, current flame retardant design strategy usually realizes satisfied flame retardancy at the expense of other properties. Herein, a novel multifunctional high-efficiency boron-containing polyphosphonamide (PB) is synthesized, and its impacts on integrated properties of EP are studied thoroughly. As expected, the well-designed PB features high flame retardant efficiency due to the combination of phosphorus, boron and nitrogen elements, only 3 wt% of which increases the limiting oxygen index (LOI) and UL-94 classification of EP thermoset to 32.2% and V-0, with a ~32.2% decrease in the peak smoke production rate (PSPR). Compared with the unmodified EP sample, the tensile strength, elongation at break and impact strength of EP sample with 3 wt% PB are elevated by ~29.8%, ~37.7% and ~50.2%, respectively. Meanwhile, high glass transmission temperature and transparency are maintained. Hence, this work offers an integrated strategy to develop highly efficient multifunctional polyphosphonamides for the preparation of high-performance flame-retardant and smoke-suppressive EPs combining high mechanical strength and toughness, thermal resistance and transparency, which are expected to meet the increasingly rigorous industrial requirements. |
| Keywords | Boron-derived polyphosphonamide; Epoxy; Flame-retardancy; Higher efficiency; Mechanical; Performance; Property; Resin samples; Smoke suppression; Thermal |
| Contains Sensitive Content | Does not contain sensitive content |
| ANZSRC Field of Research 2020 | 340302. Macromolecular materials |
| 401605. Functional materials | |
| 401602. Composite and hybrid materials | |
| 401609. Polymers and plastics | |
| Public Notes | Files associated with this item cannot be displayed due to copyright restrictions. |
| Byline Affiliations | Centre for Future Materials |
| NingboTech University, China | |
| Zhejiang University, China | |
| Institution of Origin | University of Southern Queensland |
| Funding source | Australian Research Council (ARC) Grant ID DP190102992 |
| Funding source | Australian Research Council (ARC) Grant ID FT190100188 |
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Wang, Hao and Ning, Zhiliang. 2007. "Magnesium thixotropic structure produced by controlled nucleation method ." Tezhong Zhuzao Ji Youse Hejin (Special Casting and Nonferrous Alloys).In-situ Si/Al composite produced by semisolid metal processing
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Wang, H., Estrin, Y., Fu, H. M., Song, G. L. and Zuberova, Z.. 2007. "The effect of pre-processing and grain structure on the bio-corrosion and fatigue resistance of magnesium alloy AZ31." Advanced Engineering Materials. 9 (11), pp. 967-972. https://doi.org/10.1002/adem.200700200Effects of carbon nanotubes and metal catalysts on hydrogen storage in magnesium nanocomposite
Yao, X. D., Wu, C. Z., Wang, Hao, Cheng, H. M. and Lu, G. Q.. 2006. "Effects of carbon nanotubes and metal catalysts on hydrogen storage in magnesium nanocomposite." Journal of Nanoscience and Nanotechnology. 6 (2), pp. 494-498.In situ TiB-reinforced cu-based bulk metallic glass composites
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Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2006. "In-situ Cu-based bulk metallic glass composite." International Journal of Modern Physics B. 20 (25-27), pp. 3963-3968. https://doi.org/10.1142/S0217979206040696The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy." Scripta Materialia. 55 (2), pp. 147-150. https://doi.org/10.1016/j.scriptamat.2006.03.052Modeling of semisolid structure formation in controlled nucleation method
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Wang, Hao. 2006. "In-situ Si/Al composite produced by semisolid metal processing ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "Tungsten fibre reinforced Zr-based bulk metallic glass composites ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2007. "Tungsten fibre reinforced Zr-based bulk metallic glass composites." Materials and Manufacturing Processes. 22 (5-6), pp. 687-691. https://doi.org/10.1080/10426910701384922The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ
Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao and Aravinthan, Thiru. 2010. "The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ." Goh, Steven C. and Wang, Hao (ed.) 2010 Southern Region Engineering Conference (SREC 2010). Toowoomba, Australia 11 - 12 Nov 2010 Toowoomba, Australia.Sustainable materials research at USQ
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Ning, Z. L., Wang, H., Liu, H. H., Cao, F. Y., Wang, S. T. and Sun, J. F.. 2010. "Effects of Nd on microstructures and properties at the elevated temperature of a Mg-0.3Zn-0.32Zr alloy." Materials and Design. 31 (9), pp. 4438-4444. https://doi.org/10.1016/j.matdes.2010.04.021The role of casting temperature in preparation of bulk metallic glasses
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Xu, Lihua, Fang, Zhengping, Song, Pingan and Peng, Mao. 2010. "Functionalization of carbon nanotubes by corona-discharge induced graft polymerization for the reinforcement of epoxy nanocomposites." Plasma Processes and Polymers. 7 (9), pp. 785-793. https://doi.org/10.1002/ppap.201000019Thermal degradation and flammability properties of HDPE/EVA/C60 nanocomposites
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Song, Pingan, Fang, Zhengping, Tong, Lifang and Xu, Zhongbin. 2009. "Synthesis of a novel oligomeric intumescent flame retardant and its application in polypropylene." Polymer Engineering and Science. 48 (7), pp. 1326-1331. https://doi.org/10.1002/pen.21153Fabrication of fullerene (C60) decorated carbon nanotubes and their application in flame-retarding polypropylene
Song, Pingan, Shen, Yu, Du, Baoxian, Guo, Zhenghong and Fang, Zhengping. 2009. "Fabrication of fullerene (C60) decorated carbon nanotubes and their application in flame-retarding polypropylene." Nanoscale. 1 (1), pp. 118-121. https://doi.org/10.1039/B9NR00026GEffects of reactive compatibilization on the morphological, thermal, mechanical and rheological properties of intumescent flame retarded polypropylene
Song, Pingan, Shen, Yu, Du, Baoxian, Peng, Mao, Shen, Lie and Fang, Zhengping. 2009. "Effects of reactive compatibilization on the morphological, thermal, mechanical and rheological properties of intumescent flame retarded polypropylene." ACS Applied Materials and Interfaces. 1 (2), pp. 452-459. https://doi.org/10.1021/am8001204Fabrication of dendrimer-like fullerene (C60) decorated oligomeric intumescent flame retardant for reducing the thermal oxidation and flammability of polypropylene nanocomposites
Song, Pingan, Liu, Hui, Shen, Yu, Du, Baoxian, Fang, Zhengping and Wu, Yu. 2009. "Fabrication of dendrimer-like fullerene (C60) decorated oligomeric intumescent flame retardant for reducing the thermal oxidation and flammability of polypropylene nanocomposites." Journal of Materials Chemistry. 19 (9), pp. 1305-1313. https://doi.org/10.1039/b815610gSurface-initiated graft polymerization on multiwalled carbon nanotubes pretreated by corona discharge at atmospheric pressure
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Fu, H. M., Zhang, H. F., Wang, Hao and Hu, Z. Q.. 2007. "Multifarious fracture features of CuZrAlGd(Ag) bulk metallic glasses." Advanced Materials Research. 29-30, pp. 47-50.A practical thermodynamic method to calculate the best glass-forming composition for bulk metallic glasses
Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2007. "A practical thermodynamic method to calculate the best glass-forming composition for bulk metallic glasses." International Journal of Nonlinear Sciences and Numerical Simulation. 8 (2), pp. 171-178.Effect of cooling conditions on grain size of AZ91 alloy
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Wang, Hao. 2005. "Bulk metallic glass composites." Journal of Materials Science and Technology. 21 (1 (Supplement)), pp. 86-90.Flame-retardant-wrapped carbon nanotubes for simultaneously improving the flame retardancy and mechanical properties of polypropylene
Song, Ping'an, Xu, Lihua, Guo, Zhenghong, Zhang, Yan and Fang, Zhengping. 2008. "Flame-retardant-wrapped carbon nanotubes for simultaneously improving the flame retardancy and mechanical properties of polypropylene." Journal of Materials Chemistry. 18 (42), pp. 5083-5091. https://doi.org/10.1039/b808309fC60 reduces the flammability of polypropylene nanocomposites by in situ forming gelled-ball network
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