Improved flame resistance and thermo-mechanical properties of epoxy resin nanocomposites from functionalized graphene oxide via self-assembly in water
Article
Fang, Fang, Ran, Shiya, Fang, Zhengping, Song, Pingan and Wang, Hao. 2019. "Improved flame resistance and thermo-mechanical properties of epoxy resin nanocomposites from functionalized graphene oxide via self-assembly in water." Composites Part B: Engineering. 165, pp. 406-416. https://doi.org/10.1016/j.compositesb.2019.01.086
| Article Title | Improved flame resistance and thermo-mechanical properties of epoxy resin nanocomposites from functionalized graphene oxide via self-assembly in water |
|---|---|
| ERA Journal ID | 4883 |
| Article Category | Article |
| Authors | Fang, Fang (Author), Ran, Shiya (Author), Fang, Zhengping (Author), Song, Pingan (Author) and Wang, Hao (Author) |
| Journal Title | Composites Part B: Engineering |
| Journal Citation | 165, pp. 406-416 |
| Number of Pages | 11 |
| Year | 2019 |
| Publisher | Elsevier |
| Place of Publication | United Kingdom |
| ISSN | 1359-8368 |
| Digital Object Identifier (DOI) | https://doi.org/10.1016/j.compositesb.2019.01.086 |
| Web Address (URL) | https://www.sciencedirect.com/science/article/pii/S1359836818342008 |
| Abstract | The development of a green and facile strategy for fabricating ecofriendly, highly effective flame retardants has remain a major challenge. Herein, supermolecular aggregates of piperazine (PiP) and phytic acid (PA) have been self-assembled onto the graphene oxide (GO) surface in water to fabricate functionalized GO (PPGO). The chemical structure and morphology of PPGO are determined by the X-ray photoelectron spectroscopy, transmission electron microscopy and scanning electron microscopy along with the energy dispersive spectroscopy. Due to the introduction of organic component onto the surface of graphene oxide, the adhesion between PPGO and the epoxy resin (EP) matrix is enhanced. As a result, the storage modulus (E′) of EP composites is increased in addition to a better dispersion of PPGO. Compared with the pure EP, the flame resistance of EP/PPGO is significantly improved, exhibiting a 42% decrease in peak heat release rate (pHRR), 22% reduction in total heat release (THR). The reduced flammability of EP is attributed to the synergistic effects afforded by the gas dilution effect of piperazine, char-forming promotion effect of phytic acid and the creation of 'tortuous path' barrier effect of GO during burning. This work offers a green and facile approach for creating highly effective graphene-based flame retardants. |
| Keywords | Epoxy resinP, N-containing flame retardants, Graphene oxide, Flame retardancy |
| Contains Sensitive Content | Does not contain sensitive content |
| ANZSRC Field of Research 2020 | 401605. Functional materials |
| 401609. Polymers and plastics | |
| 401602. Composite and hybrid materials | |
| Public Notes | Files associated with this item cannot be displayed due to copyright restrictions. |
| Byline Affiliations | Zhejiang University, China |
| Centre for Future Materials | |
| Institution of Origin | University of Southern Queensland |
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Yao, X. D., Wu, C. Z., Wang, Hao, Cheng, H. M. and Lu, G. Q.. 2006. "Effects of carbon nanotubes and metal catalysts on hydrogen storage in magnesium nanocomposite." Journal of Nanoscience and Nanotechnology. 6 (2), pp. 494-498.In situ TiB-reinforced cu-based bulk metallic glass composites
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Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2006. "In-situ Cu-based bulk metallic glass composite." International Journal of Modern Physics B. 20 (25-27), pp. 3963-3968. https://doi.org/10.1142/S0217979206040696The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy." Scripta Materialia. 55 (2), pp. 147-150. https://doi.org/10.1016/j.scriptamat.2006.03.052Modeling of semisolid structure formation in controlled nucleation method
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Wang, Hao. 2006. "In-situ Si/Al composite produced by semisolid metal processing ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
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Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2007. "Tungsten fibre reinforced Zr-based bulk metallic glass composites." Materials and Manufacturing Processes. 22 (5-6), pp. 687-691. https://doi.org/10.1080/10426910701384922The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ
Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao and Aravinthan, Thiru. 2010. "The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ." Goh, Steven C. and Wang, Hao (ed.) 2010 Southern Region Engineering Conference (SREC 2010). Toowoomba, Australia 11 - 12 Nov 2010 Toowoomba, Australia.Sustainable materials research at USQ
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Ning, Z. L., Wang, H., Liu, H. H., Cao, F. Y., Wang, S. T. and Sun, J. F.. 2010. "Effects of Nd on microstructures and properties at the elevated temperature of a Mg-0.3Zn-0.32Zr alloy." Materials and Design. 31 (9), pp. 4438-4444. https://doi.org/10.1016/j.matdes.2010.04.021The role of casting temperature in preparation of bulk metallic glasses
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Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2007. "A practical thermodynamic method to calculate the best glass-forming composition for bulk metallic glasses." International Journal of Nonlinear Sciences and Numerical Simulation. 8 (2), pp. 171-178.Effect of cooling conditions on grain size of AZ91 alloy
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Song, Pingan, Zhu, Yan, Tong, Lifang and Fang, Zhengping. 2008. "C60 reduces the flammability of polypropylene nanocomposites by in situ forming gelled-ball network." Nanotechnology. 19 (22). https://doi.org/10.1088/0957-4484/19/22/225707Polypropylene/clay nanocomposites prepared by in situ grafting–melt intercalation with a novel co-intercalating monomer
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Fang, Zhengping, Song, Pingan, Tong, Lifang and Guo, Zhenghong. 2008. "Thermal degradation and flame retardancy of polypropylene/C60 nanocomposites." Thermochimica Acta. 473 (1), pp. 106-108. https://doi.org/10.1016/j.tca.2008.04.019Effects of metal chelates on a novel oligomeric intumescent flame retardant system for polypropylene
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Wang, Hao, Zhang, M. X., Shi, Z. M. and Yang, Ke. 2006. "Biocorrosion behaviour of magnesium alloys under pseudo-physiological conditions." Tissue Engineering. 12 (4), pp. 1067-1067.Semisolid structure simulation in controlled nucleation process
Wang, H. and Yao, X. D.. 2006. "Semisolid structure simulation in controlled nucleation process." Solid State Phenomena. 116-117, pp. 614-617.The effect of initial microstructure of A356 alloys on the mechanical behavior in the semisolid state
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