Enhanced toughness of PLLA/PCL blends using poly(d-lactide)-poly(ε-caprolactone)-poly(d-lactide) as compatibilizer
Article
Xiao, Xianglian, Chevali, Venkata S., Song, Pingan, Yu, Bin, Yang, Yihu and Wang, Hao. 2020. "Enhanced toughness of PLLA/PCL blends using poly(d-lactide)-poly(ε-caprolactone)-poly(d-lactide) as compatibilizer." Composites Communications. 21, pp. 1-6. https://doi.org/10.1016/j.coco.2020.100385
| Article Title | Enhanced toughness of PLLA/PCL blends using poly(d-lactide)-poly(ε-caprolactone)-poly(d-lactide) as compatibilizer |
|---|---|
| ERA Journal ID | 210299 |
| Article Category | Article |
| Authors | Xiao, Xianglian (Author), Chevali, Venkata S. (Author), Song, Pingan (Author), Yu, Bin (Author), Yang, Yihu (Author) and Wang, Hao (Author) |
| Journal Title | Composites Communications |
| Journal Citation | 21, pp. 1-6 |
| Article Number | 100385 |
| Number of Pages | 6 |
| Year | 2020 |
| Publisher | Elsevier |
| Place of Publication | Netherlands |
| ISSN | 2452-2139 |
| Digital Object Identifier (DOI) | https://doi.org/10.1016/j.coco.2020.100385 |
| Web Address (URL) | https://www.sciencedirect.com/science/article/pii/S2452213920301133 |
| Abstract | Poly(l-lactide) (PLLA)/poly(ε-caprolactone) (PCL) blends traditionally show low ductility because of the immiscibility between PLLA and PCL. In this study, this ductility challenge was addressed by modifying the compatibility between PLLA and PCL using poly(d-lactide)-poly(ε-caprolactone)-poly(d-lactide) (PDLA-PCL-PDLA or PCDL) tri-block copolymer. PLLA/PCL and PLLA/PCL blends with 0.7 phr and 3.5 phr PCDL were prepared by melt-compounding and extrusion and analyzed. The compatibilized PLLA/PCL blend with 3.5 phr of PCDL exhibited an elongation-at-break of 43%, compared to 18% in uncompatibilized PLLA/PCL, although PLLA/PCL/PCDL3.5 showed the higher crystallinity of 10.0% compared to 3.1% in PLLA baseline. The stereocomplexation effect between PLLA and PDLA was confirmed with a melting peak of a stereocomplex crystallite at 212 °C through differential scanning calorimetry. PCDL compatibilization improved miscibility between PLLA and PCL as evidenced through the interfacial morphology analysis, and supported by the rheological analysis, which elucidated the enhanced melting viscosity and interfacial adhesion of PLLA/PCL. Overall, the compatibilization of PLLA/PCL blends with PCDL was effective in achieving an enhanced interfacial morphology and adhesion, and improved elongation-at-break. |
| Keywords | Poly(l-lactide); Poly(ε-caprolactone); PDLA-PCL-PDLA; Toughness; Stereocomplex; Compatibilization |
| Contains Sensitive Content | Does not contain sensitive content |
| ANZSRC Field of Research 2020 | 340399. Macromolecular and materials chemistry not elsewhere classified |
| 401602. Composite and hybrid materials | |
| Public Notes | Files associated with this item cannot be displayed due to copyright restrictions. |
| Byline Affiliations | Centre for Future Materials |
| Shenzhen Esun Industrial, China | |
| Institution of Origin | University of Southern Queensland |
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Fajrin, Jauhar, Zhuge, Yan, Bullen, Frank and Wang, Hao. 2011. "The implementation of statistical inference to study the bending strength of sustainable hybrid sandwich panel composite." Advanced Materials Research. 250-253, pp. 956-961. https://doi.org/10.4028/www.scientific.net/AMR.250-253.956Effects of fly ash source and curing procedure on strength development of geopolymers
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Kabir, M. M., Wang, H., Cardona, F. and Aravinthan, T.. 2011. "Effect of chemical treatment on the mechanical and thermal properties of hemp fibre reinforced thermoset sandwich composites." Fragomeni, Sam, Venkatesan, Srikanth, Lam, Nelson T. K. and Setunge, Sujeeva (ed.) 21st Australasian Conference on the Mechanics of Structures and Materials (ACMSM 21). Melbourne, Australia 07 - 10 Dec 2010 Leiden, Netherlands. https://doi.org/10.1201/b10571-78Mechanical properties of an injected silk fibre reinforced PLA composite
Ho, Mei-Po, Lau, Kin-tak, Wang, Hao and Bhattacharyya, Debes. 2011. "Mechanical properties of an injected silk fibre reinforced PLA composite." Bhattacharyya, D., Lin, R. J. T. and Srivatsan, T. S. (ed.) 19th International Symposium on Processing and Fabrication of Advanced Materials (PFAM XIX). Auckland, New Zealand 14 - 17 Jan 2011 Auckland, New Zealand.Flexural strength of sandwich panel with lignocellulosic composites intermediate layer: a statistic approach
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Hua, Fuan, Zhang, Chaoyi, Li, Qiang, Yu, Baoyi, Liu, Weihua, Li, Runxia, Xie, Shuisheng, Huang, Guojie, Cheng, Lei, Fu, Yao and Wang, Hao. 2011. "Numerical simulation of rolling process and microstructure evolution of AM50 Mg alloy during hot rolling process ." Advanced Materials Research. 291-294, pp. 449-454. https://doi.org/10.4028/www.scientific.net/AMR.291-294.449Deformation behaviour of aluminum alloy A356 in semisolid state
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Zhu, Z. W., Zhang, H. F., Wang, H., Ding, B. Z. and Hu, Z. Q.. 2008. "Influence of casting temperature on the thermal stability of Cu- and Zr-based metallic glasses: theoretical analysis and experiments." Journal of Materials Research. 23 (10), pp. 2714-2719. https://doi.org/10.1557/jmr.2008.0335Solidification microstructure modelling using cellular automaton method
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Fu, H. M., Qiu, D., Zhang, M. X., Wang, H., Kelly, P. M. and Taylor, J. A.. 2008. "The development of a new grain refiner for magnesium alloys using the edge-to-edge model." Journal of Alloys and Compounds. 456 (1-2), pp. 390-394. https://doi.org/10.1016/j.jallcom.2007.02.076Cu-based bulk amorphous alloy with larger glass-forming ability and supercooled liquid region
Fu, H. M., Zhang, H. F., Wang, H. and Hu, Z. Q.. 2008. "Cu-based bulk amorphous alloy with larger glass-forming ability and supercooled liquid region." Journal of Alloys and Compounds. 458 (1-2), pp. 390-393. https://doi.org/10.1016/j.jallcom.2007.03.114Study of biodegradation of pure magnesium
Ren, Yibin, Wang, Hao, Huang, Jingjing, Zhang, Bingchun and Yang, Ke. 2007. "Study of biodegradation of pure magnesium." Kim, Young-Ha, Cho, Chong-Su, Kang, Inn-Kyu, Kim, Suk Young and Kwon, Oh Hyeong (ed.) ASBM7: 7th Asian Symposium on Biomedical Materials. Jeju, Korea 20 - 23 Aug 2006 Switzerland. https://doi.org/10.4028/www.scientific.net/KEM.342-343.601The use of simulated games in an undergraduate course manufacturing processes
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Yao, Xiangdong, Wang, Hao, He, B. and Zhou, X.. 2005. "Modeling of columnar-to-equiaxed transition in solidified Al-Si alloys." Zhong, Z., Saka, H., Kim, T. H., Holm, E. A., Han, Y. and Xie, X. (ed.) 5th Pacific Rim International Conference on Advanced Materials and Processing (PRICM 5). Beijing, China 02 - 05 Nov 2004 Zurich, Switzerland. Scientific.Net. https://doi.org/10.4028/www.scientific.net/MSF.475-479.3141Formation and mechanical properties of Mg65Cu25Er10 and Mg65Cu15Ag10Er10 bulk amorphous alloys
Liu, Weili, Zhang, H. F., Hu, Z. Q. and Wang, Hao. 2005. "Formation and mechanical properties of Mg65Cu25Er10 and Mg65Cu15Ag10Er10 bulk amorphous alloys." Journal of Alloys and Compounds. 397 (1-2), pp. 202-206. https://doi.org/10.1016/j.jallcom.2005.01.043Synthesis and mechanical properties of Cu-based bulk metallic glass composites containing in-situ TiC particles
Fu, H. M., Zhang, H. F., Wang, Hao, Zhang, Qingsheng and Hu, Z. Q.. 2005. "Synthesis and mechanical properties of Cu-based bulk metallic glass composites containing in-situ TiC particles." Scripta Materialia. 52 (7), pp. 669-673. https://doi.org/10.1016/j.scriptamat.2004.10.031Preface to futures in mechanics of structures and materials conference. ACMSM20
Aravinthan, Thiru, Karunasena, Warna (Karu) and Wang, Hao. 2009. "Preface to futures in mechanics of structures and materials conference. ACMSM20." Aravinthan, Thiru, Karunasena, Warna (Karu) and Wang, Hao (ed.) 20th Australasian Conference on the Mechanics of Structures and Materials (ACMSM20). Toowoomba, Australia 02 - 05 Dec 2008 London, United Kingdom.Magnesium thixotropic structure produced by controlled nucleation method
Wang, Hao and Ning, Zhiliang. 2007. "Magnesium thixotropic structure produced by controlled nucleation method ." Tezhong Zhuzao Ji Youse Hejin (Special Casting and Nonferrous Alloys).In-situ Si/Al composite produced by semisolid metal processing
Wang, Hao. 2007. "In-situ Si/Al composite produced by semisolid metal processing." Materials and Manufacturing Processes. 22 (5-6), pp. 696-699. https://doi.org/10.1080/10426910701384963The effect of pre-processing and grain structure on the bio-corrosion and fatigue resistance of magnesium alloy AZ31
Wang, H., Estrin, Y., Fu, H. M., Song, G. L. and Zuberova, Z.. 2007. "The effect of pre-processing and grain structure on the bio-corrosion and fatigue resistance of magnesium alloy AZ31." Advanced Engineering Materials. 9 (11), pp. 967-972. https://doi.org/10.1002/adem.200700200Effects of carbon nanotubes and metal catalysts on hydrogen storage in magnesium nanocomposite
Yao, X. D., Wu, C. Z., Wang, Hao, Cheng, H. M. and Lu, G. Q.. 2006. "Effects of carbon nanotubes and metal catalysts on hydrogen storage in magnesium nanocomposite." Journal of Nanoscience and Nanotechnology. 6 (2), pp. 494-498.In situ TiB-reinforced cu-based bulk metallic glass composites
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "In situ TiB-reinforced cu-based bulk metallic glass composites." Scripta Materialia. 54 (11), pp. 1961-1966. https://doi.org/10.1016/j.scriptamat.2006.01.048In-situ Cu-based bulk metallic glass composite
Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2006. "In-situ Cu-based bulk metallic glass composite." International Journal of Modern Physics B. 20 (25-27), pp. 3963-3968. https://doi.org/10.1142/S0217979206040696The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy." Scripta Materialia. 55 (2), pp. 147-150. https://doi.org/10.1016/j.scriptamat.2006.03.052Modeling of semisolid structure formation in controlled nucleation method
Yao, X. and Wang, H.. 2006. "Modeling of semisolid structure formation in controlled nucleation method ." International Journal of Modern Physics B. 20 (25-27), pp. 4123-4128. https://doi.org/10.1142/S0217979206040969In-situ Si/Al composite produced by semisolid metal processing
Wang, Hao. 2006. "In-situ Si/Al composite produced by semisolid metal processing ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "Tungsten fibre reinforced Zr-based bulk metallic glass composites ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2007. "Tungsten fibre reinforced Zr-based bulk metallic glass composites." Materials and Manufacturing Processes. 22 (5-6), pp. 687-691. https://doi.org/10.1080/10426910701384922The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ
Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao and Aravinthan, Thiru. 2010. "The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ." Goh, Steven C. and Wang, Hao (ed.) 2010 Southern Region Engineering Conference (SREC 2010). Toowoomba, Australia 11 - 12 Nov 2010 Toowoomba, Australia.Sustainable materials research at USQ
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Zhu, Zhengwang, Zhang, Haifeng, Wang, Hao, Ding, Bingzhe, Hu, Zhuang-Qi and Huang, Han. 2009. "Influence of casting temperature on microstructures and mechanical properties of Cu50Zr45.5Ti2.5Y2 metallic glass prepared using copper mold casting [+ Erratum]." Journal of Materials Research. 24 (10), pp. 3108-3115. https://doi.org/10.1557/jmr.2009.0373Deformation behavior of semisolid A356 alloy prepared by low temperature pouring
Ning, Z. L., Wang, H. and Sun, J. F.. 2010. "Deformation behavior of semisolid A356 alloy prepared by low temperature pouring." Materials and Manufacturing Processes. 25 (7), pp. 648-653. https://doi.org/10.1080/10426910903447279Effects of Nd on microstructures and properties at the elevated temperature of a Mg-0.3Zn-0.32Zr alloy
Ning, Z. L., Wang, H., Liu, H. H., Cao, F. Y., Wang, S. T. and Sun, J. F.. 2010. "Effects of Nd on microstructures and properties at the elevated temperature of a Mg-0.3Zn-0.32Zr alloy." Materials and Design. 31 (9), pp. 4438-4444. https://doi.org/10.1016/j.matdes.2010.04.021The role of casting temperature in preparation of bulk metallic glasses
Wang, Hao. 2010. "The role of casting temperature in preparation of bulk metallic glasses ." Chandra, T., Wanderka, N., Reimers, W. and Ionescu, M. (ed.) 6th International Conference on Processing and Manufacturing of Advanced Materials (THERMEC 2009): Processing, Fabrication, Properties, Applications. Berlin, Germany 25 - 29 Aug 2009 Switzerland. https://doi.org/10.4028/www.scientific.net/MSF.638-642.1671Characteristics of a silk fibre reinforced biodegradable plastic
Ho, Mei-Po, Lau, Kin-Tak, Wang, Hao and Bhattacharyya, Debes. 2011. "Characteristics of a silk fibre reinforced biodegradable plastic." Composites Part B: Engineering. 42 (2), pp. 117-122. https://doi.org/10.1016/j.compositesb.2010.10.007Effects of natural fibre surface on composite properties: a review
Kabir, M. M., Wang, H., Aravinthan, T., Cardona, F. and Lau, K. -T.. 2011. "Effects of natural fibre surface on composite properties: a review." Cowled, Craig J. L. (ed.) 1st International Postgraduate Conference on Engineering, Designing and Developing the Built Environment for Sustainable Wellbeing (eddBE 2011). Brisbane, Australia 27 - 29 Apr 2011 Brisbane, Australia.A review on the tensile properties of natural fiber reinforced polymer composites
Ku, H., Wang, H., Pattarachaiyakoop, N. and Trada, M.. 2011. "A review on the tensile properties of natural fiber reinforced polymer composites ." Composites Part B: Engineering. 42 (4), pp. 856-873. https://doi.org/10.1016/j.compositesb.2011.01.010Cellular automaton modeling of semisolid microstructure formation
Li, Qiang, Yu, Baoyi, Zhang, Huawen, Li, Runxia, Wang, Feng, Xie, Shuisheng, Huang, Guojie and Wang, Hao. 2010. "Cellular automaton modeling of semisolid microstructure formation." China Foundry. 7 (2), pp. 143-148.Mechanical and thermal properties of untreated and chemically treated jute fibre reinforced composites
Kabir, Mohammad Mazedul, Islam, Md Mainul and Wang, Hao. 2010. "Mechanical and thermal properties of untreated and chemically treated jute fibre reinforced composites." 1st International Conference on Mechanical, Industrial and Energy Engineering (ICMIEE 2010) . Khulna, Bangladesh 23 - 24 Dec 2010 Khulna, Bangladesh.An investigation of spectral response of embedded Fibre Bragg Grating (FBG) sensors in a hollow composite cylindrical beam under pure torsion and combined loading
Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao, Followell, David, Birt, Peter, Canning, John and Stevenson, Michael. 2010. "An investigation of spectral response of embedded Fibre Bragg Grating (FBG) sensors in a hollow composite cylindrical beam under pure torsion and combined loading." Teh, Kian, Davies, Ian and Howard, Ian (ed.) 6th Australasian Congress on Applied Mechanics (ACAM 6). Perth, Western Australia 12 - 15 Dec 2010 Perth, Australia.Effects of the self distortions of embedded FBG sensors on spectral response due to torsional and combined loads
Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao and Canning, John. 2010. "Effects of the self distortions of embedded FBG sensors on spectral response due to torsional and combined loads." 3rd Asia-Pacific Workshop on Structural Health Monitoring (APWSHM 2010). Tokyo, Japan 30 Nov - 02 Dec 2010 Tokyo, Japan.Natural fibre composites with epoxidized vegetable oil (EVO) resins: a review
Manthey, N. W., Cardona, F., Aravinthan, T., Wang, H. and Cooney, T.. 2010. "Natural fibre composites with epoxidized vegetable oil (EVO) resins: a review." Goh, Steven C. and Wang, Hao (ed.) 2010 Southern Region Engineering Conference (SREC 2010). Toowoomba, Australia 11 - 12 Nov 2010 Toowoomba, Australia.Magnesium and magnesium alloys as degradable metallic biomaterials
Wang, H., Shi, Z. M. and Yang, K.. 2008. "Magnesium and magnesium alloys as degradable metallic biomaterials." Bell, John, Yan, Cheng, Ye, Lin and Zhang, Liangchi (ed.) International Conference on Frontiers in Materials Science and Technology (FMST 2008). Brisbane, Australia 26 - 28 Mar 2008 Zurich, Switzerland. https://doi.org/10.4028/www.scientific.net/AMR.32.207Study of bio-corrosion of pure magnesium
Ren, Yibin, Huang, Jingjing, Yang, Ke, Zhang, Bingchun, Yao, Zhiming and Wang, Hao. 2005. "Study of bio-corrosion of pure magnesium." Jinshu Xuebao. 41 (11), pp. 1228-1232.Present status and future trends in production of semisolid materials
Wang, Hao. 2003. "Present status and future trends in production of semisolid materials." Tezhong Zhuzao Ji Youse Hejin (Special Casting and Nonferrous Alloys). 131, pp. 332-334.Hydrogen storage of magnesium-based nanocomposites system
Yao, X., Wu, C. Z., Wang, H., Cheng, H. M. and Lu, G. Q. Max. 2005. "Hydrogen storage of magnesium-based nanocomposites system." Journal of Materials Science and Technology. 21 (1 (Supplement)), pp. 57-60.Microstructure of MmM5/Mg multi-layer hydrogen storage films prepared by magnetron sputtering
Ouyang, L. Z., Wang, Hao, Zhu, M., Zou, Jin and Chung, C. Y.. 2004. "Microstructure of MmM5/Mg multi-layer hydrogen storage films prepared by magnetron sputtering." Microscopy Research and Technique. 64 (4), pp. 323-329. https://doi.org/10.1002/jemt.20089Crystallization behavior of (Cu60Zr30Ti10)99Sn1 bulk metallic glass
Wang, Hao, Song, Xiaoping, Yao, Xiangdong, Zhang, Haifeng and Hu, Zhuangqui. 2005. "Crystallization behavior of (Cu60Zr30Ti10)99Sn1 bulk metallic glass." Journal of Materials Science and Technology. 21 (1 (Supplement)), pp. 51-53.Effects of corona discharge on the surface structure, morphology and properties of multi-walled carbon nanotubes
Xu, Lihua, Fang, Zhengping, Song, Pingan and Peng, Mao. 2010. "Effects of corona discharge on the surface structure, morphology and properties of multi-walled carbon nanotubes." Applied Surface Science. 256 (21), pp. 6447-6453. https://doi.org/10.1016/j.apsusc.2010.04.033Biodegradable aliphatic/aromatic copolymers based on terephthalic acid and poly(L-lactic acid): Synthesis, characterization and hydrolytic degradation
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Xu, Lihua, Fang, Zhengping, Song, Pingan and Peng, Mao. 2010. "Functionalization of carbon nanotubes by corona-discharge induced graft polymerization for the reinforcement of epoxy nanocomposites." Plasma Processes and Polymers. 7 (9), pp. 785-793. https://doi.org/10.1002/ppap.201000019Thermal degradation and flammability properties of HDPE/EVA/C60 nanocomposites
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Fu, Shenyuan, Song, Pingan, Yang, Haitang, Jin, Yongming, Lu, Fengzhu, Ye, Jiewang and Wu, Qiang. 2010. "Effects of carbon nanotubes and its functionalization on the thermal and flammability properties of polypropylene wood flour composites." Journal of Materials Science. 45 (13), pp. 3520-3528. https://doi.org/10.1007/s10853-010-4394-7Synthesis, characterization, and properties of degradable poly(l-lactic acid)/poly(butylene terephthalate) copolyesters containing 1,4-cyclohexanedimethanol
Wang, Bingtao, Zhang, Yan, Song, Pingan, Guo, Zhenghong, Cheng, Jie and Fang, Zhengping. 2010. "Synthesis, characterization, and properties of degradable poly(l-lactic acid)/poly(butylene terephthalate) copolyesters containing 1,4-cyclohexanedimethanol." Journal of Applied Polymer Science. 120 (5), pp. 2985-2995. https://doi.org/10.1002/app.33373Use of wireless tablet PCs as an effective learning and teaching enhancement tool
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