Synthesis of decorated graphene with P, N-containing compounds and its flame retardancy and smoke suppression effects on polylactic acid
Article
Ran, Shiya, Fang, Fang, Guo, Zhenghong, Song, Pingan, Cai, Yingfeng, Fang, Zhengping and Wang, Hao. 2019. "Synthesis of decorated graphene with P, N-containing compounds and its flame retardancy and smoke suppression effects on polylactic acid." Composites Part B: Engineering. 170, pp. 41-50. https://doi.org/10.1016/j.compositesb.2019.04.037
| Article Title | Synthesis of decorated graphene with P, N-containing compounds and its flame retardancy and smoke suppression effects on polylactic acid |
|---|---|
| ERA Journal ID | 4883 |
| Article Category | Article |
| Authors | Ran, Shiya (Author), Fang, Fang (Author), Guo, Zhenghong (Author), Song, Pingan (Author), Cai, Yingfeng (Author), Fang, Zhengping (Author) and Wang, Hao (Author) |
| Journal Title | Composites Part B: Engineering |
| Journal Citation | 170, pp. 41-50 |
| Number of Pages | 10 |
| Year | 2019 |
| Publisher | Elsevier |
| Place of Publication | United Kingdom |
| ISSN | 1359-8368 |
| Digital Object Identifier (DOI) | https://doi.org/10.1016/j.compositesb.2019.04.037 |
| Web Address (URL) | https://www.sciencedirect.com/science/article/pii/S1359836818343117 |
| Abstract | Functionalized graphene (PNFR@RGO) has been fabricated by decorating chemically reduced graphene oxide (RGO) with 9,10-dihydro-9-oxa-10-phosphaphenanthrene-10-oxide (DOPO) and branched polyethylenimine (BPEI) in this work. PNFR@RGO is then used to reduce the flammability of polylactic acid (PLA) via a melt compounding protocol. X-ray photoelectron spectroscopy (XPS) and Infrared spectroscopy (IR) have confirmed the successful fabrication of the target PNFR@RGO. The chemical decoration introduces phosphorus and nitrogen elements to the GO which can combine the formation of compact char barriers from graphene nanosheets and the elimination of free radicals when ignited or heated. The results show that the degradation temperature in air is increased and the heat release rate (HRR) is reduced. With the addition of 4 wt% PNFR@RGO, the average specific extinction area (ASEA) and the total smoke release (TSR) of PLA are noticeably suppressed by 92% and 79%, respectively. This is attributed to the combination of the corridor barrier functions of RGO and the radical-scavenging effects of PNFR. |
| Keywords | Graphene; Nanocomposites; Flame retardancy; Thermal analysis |
| Contains Sensitive Content | Does not contain sensitive content |
| ANZSRC Field of Research 2020 | 401605. Functional materials |
| 401609. Polymers and plastics | |
| 401602. Composite and hybrid materials | |
| Public Notes | Files associated with this item cannot be displayed due to copyright restrictions. |
| Byline Affiliations | Zhejiang University, China |
| Centre for Future Materials | |
| Gongniu Group, China | |
| Institution of Origin | University of Southern Queensland |
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Yao, X. D., Wu, C. Z., Wang, Hao, Cheng, H. M. and Lu, G. Q.. 2006. "Effects of carbon nanotubes and metal catalysts on hydrogen storage in magnesium nanocomposite." Journal of Nanoscience and Nanotechnology. 6 (2), pp. 494-498.In situ TiB-reinforced cu-based bulk metallic glass composites
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Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2006. "In-situ Cu-based bulk metallic glass composite." International Journal of Modern Physics B. 20 (25-27), pp. 3963-3968. https://doi.org/10.1142/S0217979206040696The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy." Scripta Materialia. 55 (2), pp. 147-150. https://doi.org/10.1016/j.scriptamat.2006.03.052Modeling of semisolid structure formation in controlled nucleation method
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Wang, Hao. 2006. "In-situ Si/Al composite produced by semisolid metal processing ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
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Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2007. "Tungsten fibre reinforced Zr-based bulk metallic glass composites." Materials and Manufacturing Processes. 22 (5-6), pp. 687-691. https://doi.org/10.1080/10426910701384922The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ
Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao and Aravinthan, Thiru. 2010. "The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ." Goh, Steven C. and Wang, Hao (ed.) 2010 Southern Region Engineering Conference (SREC 2010). Toowoomba, Australia 11 - 12 Nov 2010 Toowoomba, Australia.Sustainable materials research at USQ
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Ning, Z. L., Wang, H., Liu, H. H., Cao, F. Y., Wang, S. T. and Sun, J. F.. 2010. "Effects of Nd on microstructures and properties at the elevated temperature of a Mg-0.3Zn-0.32Zr alloy." Materials and Design. 31 (9), pp. 4438-4444. https://doi.org/10.1016/j.matdes.2010.04.021The role of casting temperature in preparation of bulk metallic glasses
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Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2007. "A practical thermodynamic method to calculate the best glass-forming composition for bulk metallic glasses." International Journal of Nonlinear Sciences and Numerical Simulation. 8 (2), pp. 171-178.Effect of cooling conditions on grain size of AZ91 alloy
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Song, Pingan, Zhu, Yan, Tong, Lifang and Fang, Zhengping. 2008. "C60 reduces the flammability of polypropylene nanocomposites by in situ forming gelled-ball network." Nanotechnology. 19 (22). https://doi.org/10.1088/0957-4484/19/22/225707Polypropylene/clay nanocomposites prepared by in situ grafting–melt intercalation with a novel co-intercalating monomer
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Fang, Zhengping, Song, Pingan, Tong, Lifang and Guo, Zhenghong. 2008. "Thermal degradation and flame retardancy of polypropylene/C60 nanocomposites." Thermochimica Acta. 473 (1), pp. 106-108. https://doi.org/10.1016/j.tca.2008.04.019Effects of metal chelates on a novel oligomeric intumescent flame retardant system for polypropylene
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Wang, Hao, Zhang, M. X., Shi, Z. M. and Yang, Ke. 2006. "Biocorrosion behaviour of magnesium alloys under pseudo-physiological conditions." Tissue Engineering. 12 (4), pp. 1067-1067.Semisolid structure simulation in controlled nucleation process
Wang, H. and Yao, X. D.. 2006. "Semisolid structure simulation in controlled nucleation process." Solid State Phenomena. 116-117, pp. 614-617.The effect of initial microstructure of A356 alloys on the mechanical behavior in the semisolid state
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