A phosphorus-containing aliphatic amine curing agent towards intrinsic flame-retardant and smoke-suppressive epoxy resins
Article
Yang, Qingshan, Wang, Jun, Yang, Shuang, Huo, Siqi, Song, Pingan, Fang, Zhengping and Wang, Hao. 2023. "A phosphorus-containing aliphatic amine curing agent towards intrinsic flame-retardant and smoke-suppressive epoxy resins." Journal of Polymer Research. 30 (2). https://doi.org/10.1007/s10965-023-03437-8
| Article Title | A phosphorus-containing aliphatic amine curing agent towards intrinsic flame-retardant and smoke-suppressive epoxy resins |
|---|---|
| ERA Journal ID | 4941 |
| Article Category | Article |
| Authors | Yang, Qingshan, Wang, Jun, Yang, Shuang, Huo, Siqi, Song, Pingan, Fang, Zhengping and Wang, Hao |
| Journal Title | Journal of Polymer Research |
| Journal Citation | 30 (2) |
| Article Number | 51 |
| Number of Pages | 11 |
| Year | 2023 |
| Place of Publication | Netherlands |
| ISSN | 1022-9760 |
| 1572-8935 | |
| Digital Object Identifier (DOI) | https://doi.org/10.1007/s10965-023-03437-8 |
| Web Address (URL) | https://link.springer.com/article/10.1007/s10965-023-03437-8 |
| Abstract | A phosphorus-containing aliphatic amine curing agent (DPT) was synthesized using triethylenetetramine (TETA) and diphenyl chlorophosphate (DPCP), and it served as a flame-retardant curing agent to reduce the fire risk of epoxy resin (EP) systems. The curing behaviors, thermal properties and flame retardancy of the DPT-containing EP systems were investigated in detail. The differential scanning calorimetry (DSC) analysis showed that the introduction of phosphorus-based group reduced the curing activity of -NH2/-NH- groups in DPT. The glass transition temperature (Tg) values of the DPT-containing EP systems were modestly lower than that of EP/TETA system. The EP cured by 29wt% DPT (EP/DPT-29) achieved a limiting oxygen index (LOI) of 27.1% and a UL-94 V-0 rating, and its peak heat release rate (PHRR) and total smoke production (TSP) were 51.6% and 37.8% lower than those of EP/TETA. The improved flame retardancy and smoke suppression of the DPT-containing EP systems was attributed to the bi-phase flame-retardant action of DPT. |
| Keywords | Aliphatic amine; Curing behaviors; Epoxy resin; Flame retardancy; Thermal properties |
| Contains Sensitive Content | Does not contain sensitive content |
| ANZSRC Field of Research 2020 | 401609. Polymers and plastics |
| Public Notes | Files associated with this item cannot be displayed due to copyright restrictions. |
| Byline Affiliations | Wuhan University of Technology, China |
| NingboTech University, China | |
| Centre for Future Materials |
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Fu, H. M., Qiu, D., Zhang, M. X., Wang, H., Kelly, P. M. and Taylor, J. A.. 2008. "The development of a new grain refiner for magnesium alloys using the edge-to-edge model." Journal of Alloys and Compounds. 456 (1-2), pp. 390-394. https://doi.org/10.1016/j.jallcom.2007.02.076Cu-based bulk amorphous alloy with larger glass-forming ability and supercooled liquid region
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Yao, X. D., Wu, C. Z., Wang, Hao, Cheng, H. M. and Lu, G. Q.. 2006. "Effects of Carbon Nanotubes and Metal Catalysts on Hydrogen Storage in Magnesium Nanocomposites." Journal of Nanoscience and Nanotechnology. 6 (2), pp. 494-498. https://doi.org/10.1166/jnn.2006.098In situ TiB-reinforced cu-based bulk metallic glass composites
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "In situ TiB-reinforced cu-based bulk metallic glass composites." Scripta Materialia. 54 (11), pp. 1961-1966. https://doi.org/10.1016/j.scriptamat.2006.01.048Numerical simulation of dendrite growth during solidification
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Wang, Hao, Fu, H. M., Zhang, H. F. and Hu, Z. Q.. 2006. "In-situ Cu-based bulk metallic glass composite." International Journal of Modern Physics B. 20 (25-27), pp. 3963-3968. https://doi.org/10.1142/S0217979206040696The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy
Fu, H. M., Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "The effect of Gd addition on the glass-forming ability of Cu-Zr-Al alloy." Scripta Materialia. 55 (2), pp. 147-150. https://doi.org/10.1016/j.scriptamat.2006.03.052Modeling of semisolid structure formation in controlled nucleation method
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Wang, Hao. 2006. "In-situ Si/Al composite produced by semisolid metal processing ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2006. "Tungsten fibre reinforced Zr-based bulk metallic glass composites ." Bandyopadhyay, Sri, Zeng, Q., Berndt, Christopher C., Rizkalla, S., Gowripalan, N. and Matison, Janison (ed.) ACUN-5 International Composites Conference. Sydney, Australia 11 - 14 Jul 2006 Sydney, Australia.Tungsten fibre reinforced Zr-based bulk metallic glass composites
Wang, Hao, Zhang, H. F. and Hu, Z. Q.. 2007. "Tungsten fibre reinforced Zr-based bulk metallic glass composites." Materials and Manufacturing Processes. 22 (5-6), pp. 687-691. https://doi.org/10.1080/10426910701384922Semisolid structure simulation in controlled nucleation process
Wang, H. and Yao, X. D.. 2006. "Semisolid structure simulation in controlled nucleation process." Solid State Phenomena. 116-117, pp. 614-617. https://doi.org/10.4028/www.scientific.net/SSP.116-117.614The effect of initial microstructure of A356 alloys on the mechanical behavior in the semisolid state
Ning, Zhiliang, Wang, Hao and Sun, Jianfei. 2006. "The effect of initial microstructure of A356 alloys on the mechanical behavior in the semisolid state." Solid State Phenomena. 116-117, pp. 449-452. https://doi.org/10.4028/www.scientific.net/SSP.116-117.449Semisolid casting of automotive component: water pump lid
Wang, Hao and Xu, Jun. 2006. "Semisolid casting of automotive component: water pump lid." Solid State Phenomena. 116-117, pp. 88-91. https://doi.org/10.4028/www.scientific.net/SSP.116-117.88The developments of structural health/integrity monitoring systems using FBG sensors at CEEFC of USQ
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Wang, Hao. 2010. "Sustainable materials research at USQ." Goh, Steven C. and Wang, Hao (ed.) 2010 Southern Region Engineering Conference (SREC 2010). Toowoomba, Australia 11 - 12 Nov 2010 Toowoomba, Australia .Deformation behavior of semisolid A356 alloy prepared by low temperature pouring
Ning, Z. L., Wang, H. and Sun, J. F.. 2010. "Deformation behavior of semisolid A356 alloy prepared by low temperature pouring." Materials and Manufacturing Processes. 25 (7), pp. 648-653. https://doi.org/10.1080/10426910903447279Effects of Nd on microstructures and properties at the elevated temperature of a Mg-0.3Zn-0.32Zr alloy
Ning, Z. L., Wang, H., Liu, H. H., Cao, F. Y., Wang, S. T. and Sun, J. F.. 2010. "Effects of Nd on microstructures and properties at the elevated temperature of a Mg-0.3Zn-0.32Zr alloy." Materials and Design. 31 (9), pp. 4438-4444. https://doi.org/10.1016/j.matdes.2010.04.021The role of casting temperature in preparation of bulk metallic glasses
Wang, Hao. 2010. "The role of casting temperature in preparation of bulk metallic glasses ." Chandra, T., Wanderka, N., Reimers, W. and Ionescu, M. (ed.) 6th International Conference on Processing and Manufacturing of Advanced Materials (THERMEC 2009): Processing, Fabrication, Properties, Applications. Berlin, Germany 25 - 29 Aug 2009 Switzerland. https://doi.org/10.4028/www.scientific.net/MSF.638-642.1671Characteristics of a silk fibre reinforced biodegradable plastic
Ho, Mei-Po, Lau, Kin-Tak, Wang, Hao and Bhattacharyya, Debes. 2011. "Characteristics of a silk fibre reinforced biodegradable plastic." Composites Part B: Engineering. 42 (2), pp. 117-122. https://doi.org/10.1016/j.compositesb.2010.10.007Effects of natural fibre surface on composite properties: a review
Kabir, M. M., Wang, H., Aravinthan, T., Cardona, F. and Lau, K. -T.. 2011. "Effects of natural fibre surface on composite properties: a review." Cowled, Craig J. L. (ed.) 1st International Postgraduate Conference on Engineering, Designing and Developing the Built Environment for Sustainable Wellbeing (eddBE 2011). Brisbane, Australia 27 - 29 Apr 2011 Brisbane, Australia.A review on the tensile properties of natural fiber reinforced polymer composites
Ku, H., Wang, H., Pattarachaiyakoop, N. and Trada, M.. 2011. "A review on the tensile properties of natural fiber reinforced polymer composites ." Composites Part B: Engineering. 42 (4), pp. 856-873. https://doi.org/10.1016/j.compositesb.2011.01.010Cellular automaton modeling of semisolid microstructure formation
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Kabir, Mohammad Mazedul, Islam, Md Mainul and Wang, Hao. 2010. "Mechanical and thermal properties of untreated and chemically treated jute fibre reinforced composites." 1st International Conference on Mechanical, Industrial and Energy Engineering (ICMIEE 2010) . Khulna, Bangladesh 23 - 24 Dec 2010 Khulna, Bangladesh.An investigation of spectral response of embedded Fibre Bragg Grating (FBG) sensors in a hollow composite cylindrical beam under pure torsion and combined loading
Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao, Followell, David, Birt, Peter, Canning, John and Stevenson, Michael. 2010. "An investigation of spectral response of embedded Fibre Bragg Grating (FBG) sensors in a hollow composite cylindrical beam under pure torsion and combined loading." Teh, Kian, Davies, Ian and Howard, Ian (ed.) 6th Australasian Congress on Applied Mechanics (ACAM 6). Perth, Western Australia 12 - 15 Dec 2010 Perth, Australia.Effects of the self distortions of embedded FBG sensors on spectral response due to torsional and combined loads
Kahandawa, Gayan C., Epaarachchi, Jayantha A., Wang, Hao and Canning, John. 2010. "Effects of the self distortions of embedded FBG sensors on spectral response due to torsional and combined loads." 3rd Asia-Pacific Workshop on Structural Health Monitoring (APWSHM 2010). Tokyo, Japan 30 Nov - 02 Dec 2010 Tokyo, Japan.Natural fibre composites with epoxidized vegetable oil (EVO) resins: a review
Manthey, N. W., Cardona, F., Aravinthan, T., Wang, H. and Cooney, T.. 2010. "Natural fibre composites with epoxidized vegetable oil (EVO) resins: a review." Goh, Steven C. and Wang, Hao (ed.) 2010 Southern Region Engineering Conference (SREC 2010). Toowoomba, Australia 11 - 12 Nov 2010 Toowoomba, Australia.Magnesium and magnesium alloys as degradable metallic biomaterials
Wang, H., Shi, Z. M. and Yang, K.. 2008. "Magnesium and magnesium alloys as degradable metallic biomaterials." Bell, John, Yan, Cheng, Ye, Lin and Zhang, Liangchi (ed.) International Conference on Frontiers in Materials Science and Technology (FMST 2008). Brisbane, Australia 26 - 28 Mar 2008 Zurich, Switzerland. https://doi.org/10.4028/www.scientific.net/AMR.32.207Present status and future trends in production of semisolid materials
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Zhu, Zhengwang, Zhang, Haifeng, Wang, Hao, Ding, Bingzhe, Hu, Zhuang-Qi and Huang, Han. 2010. "Erratum: “Influence of casting temperature on microstructures and mechanical properties of Cu50Zr45.5Ti2.5Y2 metallic glass prepared using copper mold casting” [J. Mater. Res. 24, 3108 (2009)] ." Journal of Materials Research. 25 (3), pp. 605-605. https://doi.org/10.1557/JMR.2010.0080Effects of corona discharge on the surface structure, morphology and properties of multi-walled carbon nanotubes
Xu, Lihua, Fang, Zhengping, Song, Pingan and Peng, Mao. 2010. "Effects of corona discharge on the surface structure, morphology and properties of multi-walled carbon nanotubes." Applied Surface Science. 256 (21), pp. 6447-6453. https://doi.org/10.1016/j.apsusc.2010.04.033Biodegradable aliphatic/aromatic copolymers based on terephthalic acid and poly(L-lactic acid): Synthesis, characterization and hydrolytic degradation
Wang, Bing-tao, Zhang, Yan, Song, Pingan, Guo, Zhenghong, Cheng, Jie and Fang, Zhengping. 2010. "Biodegradable aliphatic/aromatic copolymers based on terephthalic acid and poly(L-lactic acid): Synthesis, characterization and hydrolytic degradation." Chinese Journal of Polymer Science. 28 (1), pp. 405-415. https://doi.org/10.1007/s10118-010-9032-yFunctionalization of carbon nanotubes by corona-discharge induced graft polymerization for the reinforcement of epoxy nanocomposites
Xu, Lihua, Fang, Zhengping, Song, Pingan and Peng, Mao. 2010. "Functionalization of carbon nanotubes by corona-discharge induced graft polymerization for the reinforcement of epoxy nanocomposites." Plasma Processes and Polymers. 7 (9), pp. 785-793. https://doi.org/10.1002/ppap.201000019Thermal degradation and flammability properties of HDPE/EVA/C60 nanocomposites
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Song, Pingan, Fang, Zhengping, Tong, Lifang and Xu, Zhongbin. 2009. "Synthesis of a novel oligomeric intumescent flame retardant and its application in polypropylene." Polymer Engineering and Science. 48 (7), pp. 1326-1331. https://doi.org/10.1002/pen.21153Fabrication of fullerene (C60) decorated carbon nanotubes and their application in flame-retarding polypropylene
Song, Pingan, Shen, Yu, Du, Baoxian, Guo, Zhenghong and Fang, Zhengping. 2009. "Fabrication of fullerene (C60) decorated carbon nanotubes and their application in flame-retarding polypropylene." Nanoscale. 1 (1), pp. 118-121. https://doi.org/10.1039/B9NR00026GEffects of reactive compatibilization on the morphological, thermal, mechanical and rheological properties of intumescent flame retarded polypropylene
Song, Pingan, Shen, Yu, Du, Baoxian, Peng, Mao, Shen, Lie and Fang, Zhengping. 2009. "Effects of reactive compatibilization on the morphological, thermal, mechanical and rheological properties of intumescent flame retarded polypropylene." ACS Applied Materials and Interfaces. 1 (2), pp. 452-459. https://doi.org/10.1021/am8001204Fabrication of dendrimer-like fullerene (C60) decorated oligomeric intumescent flame retardant for reducing the thermal oxidation and flammability of polypropylene nanocomposites
Song, Pingan, Liu, Hui, Shen, Yu, Du, Baoxian, Fang, Zhengping and Wu, Yu. 2009. "Fabrication of dendrimer-like fullerene (C60) decorated oligomeric intumescent flame retardant for reducing the thermal oxidation and flammability of polypropylene nanocomposites." Journal of Materials Chemistry. 19 (9), pp. 1305-1313. https://doi.org/10.1039/b815610gSurface-initiated graft polymerization on multiwalled carbon nanotubes pretreated by corona discharge at atmospheric pressure
Xu, Lihua, Fang, Zhengping, Song, Pingan and Peng, Mao. 2009. "Surface-initiated graft polymerization on multiwalled carbon nanotubes pretreated by corona discharge at atmospheric pressure." Nanoscale. 2 (3), pp. 389-393. https://doi.org/10.1039/B9NR00222GDevelopment of bulk metallic glass composites
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Fu, H. M., Zhang, H. F., Wang, Hao and Hu, Z. Q.. 2007. "Multifarious fracture features of CuZrAlGd(Ag) bulk metallic glasses." Advanced Materials Research. 29-30, pp. 47-50.Effect of pouring temperature on thixotropic microstructure formation of AZ91
Ning, Zhiliang, Wu, Peilian, Wang, Hao, Cao, Fuyang and Sun, Jianfei. 2007. "Effect of pouring temperature on thixotropic microstructure formation of AZ91." Rare Metals. 26 (S1), pp. 180-184.Flame-retardant-wrapped carbon nanotubes for simultaneously improving the flame retardancy and mechanical properties of polypropylene
Song, Ping'an, Xu, Lihua, Guo, Zhenghong, Zhang, Yan and Fang, Zhengping. 2008. "Flame-retardant-wrapped carbon nanotubes for simultaneously improving the flame retardancy and mechanical properties of polypropylene." Journal of Materials Chemistry. 18 (42), pp. 5083-5091. https://doi.org/10.1039/b808309fC60 reduces the flammability of polypropylene nanocomposites by in situ forming gelled-ball network
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Fang, Zhengping, Song, Pingan, Tong, Lifang and Guo, Zhenghong. 2008. "Thermal degradation and flame retardancy of polypropylene/C60 nanocomposites." Thermochimica Acta. 473 (1), pp. 106-108. https://doi.org/10.1016/j.tca.2008.04.019Effects of metal chelates on a novel oligomeric intumescent flame retardant system for polypropylene
Song, Pingan, Fang, Zhengping, Tong, Lifang, Jin, Yongming and Lu, Fengzhu. 2008. "Effects of metal chelates on a novel oligomeric intumescent flame retardant system for polypropylene." Journal of Analytical and Applied Pyrolysis. 82 (2), pp. 286-291. https://doi.org/10.1016/j.jaap.2008.04.008Anomalous grain coarsening behaviour observed in grain-refined aluminium alloy cast using low superheat
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Wang, Hao, Davidson, C. J. and StJohn, David H.. 2004. "Semisolid microstructural evolution of AlSi7Mg during partial remelting." Materials Science and Engineering A: Structural Materials: Properties, Microstructure and Processing. 368 (1-2), pp. 159-167. https://doi.org/10.1016/j.msea.2003.10.305Biocorrosion behaviour of magnesium alloys under pseudo-physiological conditions
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